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Automated solid phase extraction

机译:自动固相萃取

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摘要

Modern analytical techniques such as LC/MS have extremely high sensitivity,reproducibility and accuracy.The overall reliability of an analytical method however depends not only on the method itself but also on the reproducibility of any pre-analytical sample preparation procedures that may be needed.Solid phase extraction (SPE) is the technique of choice for such sample preparation which is frequently necessary with samples which have complex background matrices,such as food products.Manual SPE methods are labour-intensive and can have poor reproducibility so the recent development of an automatic SPE system promises to be of significant advantage in the analysis of food samples.This report describes the use of such an automatic SPE system in the analysis of antibiotics in food.
机译:LC / MS等现代分析技术具有极高的灵敏度,可重复性和准确性。然而,分析方法的整体可靠性不仅取决于方法本身,还取决于可能需要的任何分析前样品制备程序的可重复性。固相萃取(SPE)是此类样品制备的一种选择技术,这对于具有复杂背景基质的样品(例如食品)经常是必需的。手动SPE方法劳动强度大且重现性差,因此近来的发展自动SPE系统有望在食品样品分析中具有显着优势。本报告介绍了这种自动SPE系统在食品中抗生素分析中的使用。

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