(4Z)-4-(2-Oxo­propyl­­idene)-1,3-bis­­(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one

Jihad Sebhaoui; Youness El Bakri; Ibtissam RayniKhadija El BourakadiEl Mokhtar EssassiJoel T. Mague

首页> 外文期刊>IUCrData >(4Z)-4-(2-Oxopropylidene)-1,3-bis(prop-2-en-1-yl)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one

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(4Z)-4-(2-Oxopropylidene)-1,3-bis(prop-2-en-1-yl)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one

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摘要

In the title compound, C18H20N2O2, the diazepin-2-one ring adopts a tub conformation. The conformation of the acetyl group is partially determined by an intramolecular N—HO hydrogen bond. In the crystal, pairwise C—HO hydrogen bonds form inversion dimers.

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《IUCrData》 |2017年第4期|共页
作者
Jihad Sebhaoui; Youness El Bakri; Ibtissam RayniKhadija El BourakadiEl Mokhtar EssassiJoel T. Mague;
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作者单位

Laboratoire de Chimie Organique Hétérocyclique, URAC 21, Pôle de Compétence Pharmacochimie, Av Ibn Battouta, BP 1014, Faculté des Sciences, Mohammed V University, Rabat, Morocco;

Department of Chemistry, Tulane University, New Orleans, LA 70118, USA;

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正文语种英语
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crystal structure; hydrogen bond; diazepine; crystal structure.;

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1. 6,7,6′,7′-Tetraphenyl-2,2′-bi[1,3-dithia-5,8-diazacyclopenta[b]naphthalenylidene] chloroform disolvate [J] . Bolligarla R., Das S.K., Durgaprasad G. Acta Crystallographica Section E: Crystallographic Communications . 2011,第9期

机译：6,7,6′,7′-Tetraphenyl-2,2′-bi[1,3-dithia-5,8-diazacyclopenta[b]naphthalenylidene] chloroform disolvate
2. (3R,4Z)-1,3-Diethyl-4-(2-oxo-propyl-idene)-2,3,4,5-tetra-hydro-1H-1,5-benzodiazepin-2-one [J] . El Foujji L., Sebhaoui J., El Bakri Y., IUCrData . 2018,第4期

机译：（3R，4Z）-1,3-二乙基-4-（2-氧代丙基 - 偶联）-2,3,4,5-氢丙烯-1H-1,5-苯并二氮嘧啶-2-一
3. (4Z)-4-(2-Oxo-propyl--idene)-1,3-bis--(prop-2-en-1-yl)-2,3,4,5-tetra-hydro-1H-1,5-benzodiazepin-2-one [J] . Jihad Sebhaoui, Youness El Bakri, Ibtissam Rayni, IUCrData . 2017,第4期

机译：（4Z）-4-（2-氧代丙基丙二烯）-1,3-双-（丙-2-烯-1-基）-2,3,4,5-四氢-1H- 1,5-苯并二氮杂-2-酮
4. Synthesis and thermal analysis of nanocomplexe with Erbium, mesoionic 2-(4-chlorophenyl)-3-methyl-4-(4-methylphenyl)-1,3-thiazolium-5-thiolate and Bipyridine: prospect of a biotechnological application in health [C] . Gabriela Brasileiro Campos Mota, Crislene Morais, Ana Paula Alves Barros, Annual Conference of the North American Thermal Analysis Society . 2013

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5. Bis(N′-{(E)-(2E)-13-diphenylprop-2-en-1-ylideneamino}-N-ethylcarbamimidothioato-κ2N′S)zinc(II): crystal structure and Hirshfeld surface analysis [O] . Ming Yueh Tan, Karen A. Crouse, Thahira B. S. A. Ravoof, 2017

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6. 4-{[(4Z)-5-Oxo-2-phenyl-4,5-dihydro-1,3-oxazol-4-ylidene]methyl}phenyl acetate [O] . Baldaniya, Bharat B., Jotani, Mukesh M., Tiekink, Edward R. T. 2010

机译：4-{[（（4Z）-5-Oxo-2-phenyl-4,5-dihydro-1,3-oxazol-4-yl-4-idene] meth] yl}乙酸乙酸酯
7. 1,1,3,3-Tetramethyl-2,2,4,4-Tetrakis(Trimethylsilyl)-1,3- Disilacyclobutane and Its 1,3-Digerma and 1,3-Distanna Analogs: Unexpected Products from the Reaction of Bis-(Trimethylsilyl)Bromomethyllithium with Dimethyldihalo Derivatives of Silicon, Germanium and Tin. [R] . Seyferth, D., Lefferts, J. L. 1976

机译：1,1,3,3-四甲基-2,2,4,4-四（三甲基甲硅烷基）-1,3-二硅杂环丁烷及其1,3-Digerma和1,3-Distanna类似物：来自Bis反应的意外产物 - （三甲基甲硅烷基）溴甲基锂与硅，锗和锡的二甲基二卤代衍生物。

(4Z)-4-(2-Oxo­propyl­­idene)-1,3-bis­­(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one

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(4Z)-4-(2-Oxopropylidene)-1,3-bis(prop-2-en-1-yl)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one