Thionation of tetrakis[(ethoxycarbonyl)methoxy]tetrathiacalix[4]arenes with Lawesson's reagent

Omran A. Omran; Kim L. Larsen; Reinhard Wimmer

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Thionation of tetrakis[(ethoxycarbonyl)methoxy]tetrathiacalix[4]arenes with Lawesson's reagent

机译：用Lawesson试剂对四[（乙氧羰基）甲氧基]四硫杂杯[4]芳烃进行亚硫酰化

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Tetra- and tri-thioated derivatives of tetra-kis[(ethoxycarbonyl)methoxy]tetraihiacalixf4]arenes were synthesized by thionation with Lawesson's reagent in dry toluene. The prepared compounds' structures were investigated by FT-IR, ~1H NMR, 2D-NMR, MALDI-TOF-MS, and X-ray crystallography.

机译：通过在干甲苯中使用Lawesson试剂进行硫磺化反应，合成了四-[（乙氧羰基）甲氧基]四硫代lix啶[4]芳烃的四硫代和三硫代衍生物。通过FT-IR，〜1H NMR，2D-NMR，MALDI-TOF-MS和X射线晶体学研究制备的化合物的结构。

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《Monatshefte fur Chemie》 |2008年第9期|共6页
作者
Omran A. Omran; Kim L. Larsen; Reinhard Wimmer;
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正文语种 eng
中图分类化学;
关键词
Calixarene; Thiacalixarene; Lawesson's reagent; Thionation; Synthesis;

机译：杯芳烃;噻吨芳烃;Lawesson试剂;硫磺化;合成;

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1. Thionation of tetrakis[(ethoxycarbonyl)methoxy]tetrathiacalix[4]arenes with Lawesson ’s reagent [J] . Omran A. Omran, Kim L. Larsen, Reinhard Wimmer, Monatshefte für Chemie / Chemical Monthly . 2008,第9期

机译：用Lawesson试剂对四[（乙氧羰基）甲氧基]四硫杂杯[4]芳烃进行亚硫酰化
2. Synthesis and solid state structural analysis of conformers of tetrakis((ethoxycarbonyl)methoxy)tetrathiacalix[4]arene [J] . Akdas H., Graf E., Hosseini MW., Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 1999,第11期

机译：四（（乙氧羰基）甲氧基）四硫杂杯[4]芳烃构象异构体的合成及固态结构分析
3. Aminolysis of p-tert-Butyl-tetrakis-[(ethoxycarbonyl)methoxy]thiacalix[4]arene [J] . Yan Jin, Chunlei Zhang, Shuling Gong, Synthetic Communications . 2005,第24期

机译：对叔丁基-四-[[（乙氧羰基）甲氧基]硫杂杯[4]芳烃的氨解
4. Studies on The Reactions of Cyclic Oxalyl Compounds with Oxindole and Lawesson Reagent [C] . Elif KORKUSUZ, Ismail YILDIRIM European Symposium on Organic Chemistry . 2009

机译：氧吲哚和法律试剂的环状氧基氧基化合物的反应研究
5. Amplification of N-Halo Reagent Electrophilicity by Organic Dye Organocatalysts for the Halogenation of Arenes and Heteroarenes [D] . Rogers, David A. 2020

机译：用有机染料有机催化剂扩增N-卤素试剂亲热性，用于芳烃和杂种的卤化
6. A chromatography-free and aqueous waste-free process for thioamide preparation with Lawesson’s reagent [O] . Ke Wu, Yichen Ling, An Ding, 2021

机译：无硫代酰胺的无硫代酰胺的试剂的无色谱和无含水废物的方法
7. N,N,N-Triethylethanaminium 5,11,17,23-tetra-tert-butyl-25-[(ethoxycarbonyl)methoxy]-26,28-dihydroxy-27-oxido-2,8,14,20-tetrathiacalix[4]arene: a molecular salt [O] . Joel T. Mague, Mehmet Akkurt, Shaaban K. Mohamed, 2016

机译：N，N，N-三乙基乙胺5,11,17,23-四叔丁基-25 - [（乙氧羰基）甲氧基] -26,28-二羟基-27-氧化-2,8,14,20-四硫杂[ 4]芳烃：分子盐

Thionation of tetrakis[(ethoxycarbonyl)methoxy]tetrathiacalix[4]arenes with Lawesson's reagent

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