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Nanocrystalline Ni_3Al-type intermetallic phase powder from Ni-base superalloys

机译:镍基高温合金纳米晶Ni_3Al型金属间相粉末

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摘要

Nanoscale particles of Ni_3Al-type intermetallic phase have been produced by extracting precipitates from Ni-base superalloys. The process is flexible and can be easily manipulated to tailor particle size and composition. Further, it can be readily adopted to produce nanoparticles of many other intermetallic phases with diverse compositions. The Ni_3Al-type nanopowder (approx 100 nm particle size) was characterized by x-ray diffraction and electron microscopy and compared with a micropowder (approx 450 nm particle size). The nanopowder shows enhanced specific magnetization and a slight increase in Curie temperature relative to the micropowder. This change is possibly due to small changes in composition rather than to the reduction in particle size.
机译:Ni_3Al型金属间相的纳米级颗粒是通过从镍基高温合金中提取沉淀物而产生的。该方法是灵活的,并且可以容易地操纵以调整粒度和组成。此外,可以容易地采用它来生产具有不同组成的许多其他金属间相的纳米颗粒。通过X射线衍射和电子显微镜表征Ni_3Al型纳米粉末(约100nm的粒径),并与微粉(约450nm的粒径)进行比较。相对于微粉,纳米粉表现出增强的比磁化强度和居里温度的轻微升高。该变化可能是由于组成的微小变化,而不是由于粒径的减小。

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