Domino assembly of functionalized cyclopentenols from 1,5-diphenylpentane-1,5-dione and phenylacetylene in the KOH/DMSO suspension

Trofimov Boris A.; Schmidt Elena Yu.; Bidusenko Ivan A.; Cherimichkina Natalia A.

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Domino assembly of functionalized cyclopentenols from 1,5-diphenylpentane-1,5-dione and phenylacetylene in the KOH/DMSO suspension

机译：在KOH / DMSO悬浮液中由1,5-二苯-1,5-二酮和苯乙炔官能化的环戊烯醇的多米诺组装

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摘要

1,5-Diphenylpentane-1,5-dione reacts (50 mol% KOH in DMSO, 70 degrees C, 3 h) with phenylacetylene in a domino manner to afford 3-benzoyl-2-benzyl-l-phenylcyclopenten-1-ol and its debenzoylated derivative in 66 and 25% yields, respectively.

机译：1,5-二苯基戊烷-1,5-二酮（在DMSO中为50 mol％KOH，70°C，3小时）与多聚乙炔以苯胺的方式反应，得到3-苯甲酰基-2-苄基-1-苯基环戊烯-1-醇及其脱苯甲酰化衍生物的产率分别为66％和25％。

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《Mendeleev Communications 》 |2015年第1期| 共2页
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Trofimov Boris A.; Schmidt Elena Yu.; Bidusenko Ivan A.; Cherimichkina Natalia A.;
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1. Domino assembly of functionalized cyclopentenols from 1,5-diphenylpentane-1,5-dione and phenylacetylene in the KOH/DMSO suspension [J] . Trofimov Boris A., Schmidt Elena Yu., Bidusenko Ivan A., Mendeleev Communications . 2015 ,第1期

机译：在KOH / DMSO悬浮液中由1,5-二苯-1,5-二酮和苯乙炔官能化的环戊烯醇的多米诺组装
2. 15-[(Z)-Phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecanes: stereoselective one-pot assembly from cyclohexanones and phenylacetylene in a KOH/DMSO suspension [J] . Elena Yu Schmidt, Nadezhda V. Zorina, Elena V. Skitaltseva Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2011 ,第29期

机译：15-[（Z）-苯基亚甲基] -7,14-二恶二螺[5.1.5.2]十五烷：在KOH / DMSO悬浮液中由环己酮和苯乙炔组成的立体选择性一锅组装
3. Polycyclic bridgehead acetals with enol functionality: one-pot assembly from aliphatic ketones and acetylene in KOH/DMSO suspension [J] . Schmidt Elena Yu., Bidusenko Ivan A., Cherimichkina Natalia A., Tetrahedron . 2016 ,第30期

机译：具有烯醇功能的多环桥头缩醛：在KOH / DMSO悬浮液中由脂肪族酮和乙炔一锅组装
4. Functional, degradable polyester materials synthesized from poly(ϵ-caprolactone-co-2-oxepane-1,5-dione): An investigation into the derivatization, self assembly, and degradation behavior of poly(ϵ-caprolactone)-based materials [D] . Iha, Rhiannon K. 2010

机译：由聚（ε-己内酯-co-2-环氧庚烷-1,5-二酮）合成的功能性可降解聚酯材料：基于聚（ε-己内酯）的材料的衍生化，自组装和降解行为的研究
5. Self-Assembly of NPhenyl-2,5-dimethylpyrrole from Acetylene and Aniline in KOH/DMSO and KOBut/DMSO Superbase Systems: A Quantum-Chemical Insight [O] . -1

机译：在KOH / DMSO和Kobut / DMSOS Systems中的乙炔和苯胺的Nphenyl-2,5-二甲基吡咯的自组装：量子化学洞察力

Domino assembly of functionalized cyclopentenols from 1,5-diphenylpentane-1,5-dione and phenylacetylene in the KOH/DMSO suspension

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