Preparation of N-phenyl-p-phenylenediamine by coupling of aniline and nitrobenzene in KOH-poly(ethylene glycol) medium

Babkin Alexander V.; Asachenko Andrey F.; Uborsky Dmitry V.; Kononovich Dmitry S.; Izmer Vyatcheslav V.; Kudakina Vera A.; Shnaider Viktoriya A.; Shevchenko Nikolay E.; Voskoboynikov Alexander Z.

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Preparation of N-phenyl-p-phenylenediamine by coupling of aniline and nitrobenzene in KOH-poly(ethylene glycol) medium

机译：苯胺和硝基苯在KOH-聚乙二醇介质中偶联制备N-苯基-对苯二胺

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A novel protocol for efficient coupling of nitrobenzene and aniline in poly(ethylene glycol) medium in the presence of KOH giving diphenylamine derivatives has been developed, to enable the exclusion of the toxic tetramethylammonium hydroxide catalyst commonly used in the rubber anti-degradant industry.

机译：已经开发出一种新的方案，用于在KOH存在下在聚乙二醇介质中有效地偶联硝基苯和苯胺，得到二苯胺衍生物，以排除橡胶抗降解工业中常用的有毒四甲基氢氧化铵催化剂。

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《Mendeleev Communications》 |2016年第6期|共3页
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Babkin Alexander V.; Asachenko Andrey F.; Uborsky Dmitry V.; Kononovich Dmitry S.; Izmer Vyatcheslav V.; Kudakina Vera A.; Shnaider Viktoriya A.; Shevchenko Nikolay E.; Voskoboynikov Alexander Z.;
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1. Preparation of N-phenyl-p-phenylenediamine by coupling of aniline and nitrobenzene in KOH-poly(ethylene glycol) medium [J] . Babkin Alexander V., Asachenko Andrey F., Uborsky Dmitry V., Mendeleev Communications . 2016,第6期

机译：苯胺和硝基苯在KOH-聚乙二醇介质中偶联制备N-苯基-对苯二胺
2. Preparation of metallic bismuth by reduction of bismuth formates in ethylene glycol medium [J] . Kseniya V. Mishchenko, Yurii M. Yukhin MATEC Web of Conferences . 2021,第a期

机译：通过在乙二醇介质中还原甲甲酸酯的制备金属铋
3. Ethylene glycol and H2SO4 / SiO2 as a green medium for the preparation of quinoxaline derivatives at room temperature [J] . Mozhgan Bashirzadeh, Farahnaz Kargar Behbahani European Chemical Bulletin . 2020,第1期

机译：乙二醇和H2SO4 / SiO2作为在室温下制备喹喔啉衍生物的绿色培养基
4. Preparation and magnetic properties of nickel nanowires by reduction in ethylene glycol medium under the influence of magnetic field [C] . Wanshuo Sun, Junsheng Cheng, Lankai Li International Conference on New Material and Chemical Industry . 2017

机译：磁场影响下乙二醇介质降低镍纳米线的制备和磁性
5. I. Diamino telechelic polybutadienes: Synthesis, characterization and melt coupling. II. Poly(epsilon-caprolactone-beta-poly(ethylene glycol) polymeric nanoparticles for drug delivery. III. Zirconia based cellulosic HPLC chiral stationary phase for enantioseparations. [D] . Ji, Shengxiang. 2006

机译：I.二氨基远螯聚丁二烯：合成，表征和熔融偶联。二。用于药物递送的聚（ε-己内酯-β-聚（乙二醇）聚合物纳米颗粒）III。用于对映体分离的基于氧化锆的纤维素HPLC手性固定相。
6. Docetaxel-Loaded Mixed Micelles and Polymersomes Composed of Poly (caprolactone)-Poly (ethylene glycol) (PEG-PCL) and Poly (lactic acid)-Poly (ethylene glycol) (PEG-PLA): Preparation and In-vitro Characterization [O] . Elham Khodaverdi, Zahra Tayarani-Najaran, Elham Minbashi, 2019

机译：聚己内酯-聚乙二醇（PEG-PCL）和聚（乳酸）-聚乙二醇（PEG-PLA）组成的多西他赛负载混合胶束和聚合物囊泡：制备和体外表征
7. Preparation and Characterizations of RSPP050-Loaded Polymeric Micelles Using Poly(ethylene glycol)-b-Poly(ε-caprolactone) and Poly(ethylene glycol)-b-Poly(D,L-lactide) [O] . Komgrit Eawsakul, Panarin Chinavinijkul, Rungnapha Saeeng, 2017

机译：使用聚（乙二醇） - β-i> B -pold（ε-己内酯）和聚（乙二醇） - B -poly（d ，L-丙交酯）

Preparation of N-phenyl-p-phenylenediamine by coupling of aniline and nitrobenzene in KOH-poly(ethylene glycol) medium

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