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Stacking faults of metastable gamma'' phase precipitated in an Ni-15Cr-8Fe-6Nb alloy

机译:Ni-15Cr-8Fe-6Nb合金中析出的亚稳态γ''相的堆垛层错

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The stacking faults of a metastable gamma '' phase precipitated in a nickel base superalloy, a modified JIS NCF 3 type alloy (X-750M), are investigated by TEM and an X-ray diffraction method. The gamma '' precipitates ale circular shaped plates at the early stage of aging and they become elliptic or irregular shaped plates at the latter stage of aging al temperatures up to 1033 K. Contrast which suggests the existence of stacking faults on {112}(gamma '') planes can be seen in many of the large gamma '' precipitates extracted from the specimens aged at 1033 K for 36 ks or more. It is clear that the values of gamma-gamma '' lattice mismatch increase with increasing aging time from the measurement of lattice constants of the gamma and the gamma '' phases. The formation of stacking faults on {112}(gamma '') planes in the large gamma '' precipitates is due to the movement of an a/6 [11 (1) over bar] partial dislocation introduced by gamma ''-gamma coherency strain. Since a part of the stacking sequence has a similar crystal structure to that of stable delta phase precipitates in a gamma phase, the formation of stacking faults in the gamma '' precipitates is considered to behaviour able for their stabilisation. (C) The Institute of Materials.
机译:通过TEM和X射线衍射法研究了在镍基高温合金,一种改良的JIS NCF 3型合金(X-750M)中析出的亚稳态γ''相的堆垛层错。 γ”在老化的早期阶段沉淀出圆形的平板,而在温度高达1033 K的老化的后期,它们变成椭圆形或不规则形状的平板。对比表明{112}(gamma '')在从1033 K老化36 ks或以上的样品中提取的许多大γ沉淀物中可以看到平面。显然,通过测量γ相和γ′相的晶格常数,γ-γ′晶格失配的值随着老化时间的增加而增加。大γ''沉淀物中{112}(γ'')平面上的堆积断层的形成是由于γ''-γ相干性引起的a / 6 [11(1)over bar]部分位错的运动应变。由于部分堆积序列具有与伽马相中稳定的δ相沉淀相似的晶体结构,因此认为γ沉淀中堆积缺陷的形成能够稳定它们。 (C)材料研究所。

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