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An attempt to detect SCC by combined measurements of electrochemical noise and acoustic emission

机译:尝试通过电化学噪声和声发射的组合测量来检测SCC

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摘要

Electrochemical voltage and current noise (EN) were measured simultaneously with acoustic emission (AE) during intergranular stress-corrosion cracking (IGSCC) on tensile specimens under a constant load. The elongation of the test specimens was also measured continuously during the tests, as an additional measuring technique. The test specimens were made from sensitized stainless steel of type 304, and immersed in an aqueous solution of sodium thiosulphate. The main aim of our work was to find out how successfully IGSCC processes could be detected by the simultaneous use of all three measurement methods. The results of the tests indicated that the accumulation of cracking and dissolution events could be satisfactorily monitored, whereas it was not possible to detect individual IGSCC events with the existing measuring set-up. It is not clear whether this inability to detect single IGSCC events was a consequence of the continuous nature of the IGSCC processes, or whether it was due to the insufficient resolution of the measurement system set-up.
机译:在恒定载荷下,在拉伸试样的晶间应力腐蚀开裂(IGSCC)期间,同时测量了电化学电压和电流噪声(EN)和声发射(AE)。作为一种附加的测量技术,在测试过程中还连续测量了试样的伸长率。测试样品由304型敏化不锈钢制成,并浸入硫代硫酸钠水溶液中。我们工作的主要目的是找出同时使用所有三种测量方法可以成功检测到IGSCC过程的方法。测试结果表明,可以令人满意地监测开裂和溶解事件的累积,而使用现有的测量装置不可能检测到单独的IGSCC事件。目前尚不清楚这种无法检测单个IGSCC事件的原因是IGSCC过程的连续性质的结果,还是由于测量系统设置的分辨率不足而引起的。

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