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Fabrication and Characterization of Polystyrene/Gold Nanoparticle Composite Nanofibers

机译:聚苯乙烯/金纳米颗粒复合纳米纤维的制备与表征

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Polystyrene/gold nanoparticle (PS/AuNP) composite fibers were fabricated using an electrospinning technique.Transmission electron microscopy (TEM) showed that the diameters of the naphthalenethiol-capped gold nanoparticles (prior to incorporation into the PS fibers) ranged from 2 to 5 nm.UV-vis spectroscopy revealed the surface plasmon peaks of the gold nanoparticles centered at approximately 512 nm,indicating that nano-sized Au particles are well-dispersed in solution.This was consistent with the TEM observations.The electrospun nanofibers of PS/AuNP composites were approximately 60-3,000 nm in diameter.The surface morphology of the PS/AuNP composite and the dispersability of the Au nanoparticles inside of PS after electrospinning process were investigated by SEM and TEM.The thermal behavior of the pure PS and PS/AuNP nanocomposites and fibers were examined by DSC.
机译:采用静电纺丝技术制备了聚苯乙烯/金纳米颗粒(PS / AuNP)复合纤维,透射电子显微镜(TEM)表明,萘硫醇包覆的金纳米颗粒(在掺入PS纤维之前)的直径为2至5 nm紫外可见光谱显示金纳米颗粒的表面等离激元峰集中在约512 nm处,表明纳米级的金颗粒在溶液中分散良好,这与TEM观察结果一致.PS / AuNP复合材料的电纺纳米纤维直径约为60-3,000 nm。通过SEM和TEM研究了PS / AuNP复合材料的表面形态和静电纺丝后PS内部Au纳米颗粒的分散性。纯PS和PS / AuNP纳米复合材料的热行为并且通过DSC检查纤维。

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