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The Effects of Sintering Temperature on the Physical and Electrical Properties of SrTiO3 Ceramics Prepared Via Sol-Gel Combustion Method

机译:烧结温度对溶胶-凝胶燃烧法制备SrTiO3陶瓷物理和电学性能的影响

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摘要

The SrTiO3 ceramics was prepared via sol-gel combustion method by using citric acid as a fuel. Cubic perovskite structures of SrTiO3 were obtained at 600 degrees C. The SrTiO3 powder was compacted into disks under pressure of 110 MPa, the pellets were sintered at 900-1300 degrees C and the dwelling times were variable. The result shows that the density grain size and dielectric constant increased corresponding with the increasing of dwelling times. The grain size was about 124-300 nm. The SrTiO3 sintered at 1300 degrees C for 4 h shows the highest dielectric constant (epsilon(r) = 382), dielectric loss tangent (tan delta < 0.5) and the density was about 4.42 g/cm(3).
机译:以柠檬酸为燃料,通过溶胶-凝胶燃烧法制备了SrTiO3陶瓷。在600摄氏度下获得SrTiO3的立方钙钛矿结构。在110 MPa的压力下将SrTiO3粉末压实成圆盘,在900-1300摄氏度下烧结颗粒,并改变保压时间。结果表明,随着停留时间的增加,密度晶粒尺寸和介电常数增大。晶粒尺寸为约124-300nm。在1300摄氏度下烧结4 h的SrTiO3表现出最高的介电常数(ε= 382),介电损耗角正切(tanδ<0.5)和密度约为4.42 g / cm(3)。

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