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Studies of Electrospinning Process of Zirconia Nanofibers

机译:氧化锆纳米纤维的静电纺丝工艺研究

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Eletriospinning process was used to fabricate Zirconia nanofibers and polyvinyl pyrrolidone (PVP) was employed in this procedure. SEM, TGA, FT-IR and XRD were used to investigate the electrospinning process. Pure PVP was electrospun at the same conditions as comparisons. The results indicated that the fibers had an average diameter about 80 nm with smooth surface. FT-IR spectrum and TGA curve proved that PVP was removed from the fibers after a thermal treatment. -It was found that the crystal structure of Zirconia changed at different calcination temperature. The use of PVP, bicomponent solvent of water and ethanol and inorganic salt had positive effects on the morphology of the fibers.
机译:使用电纺丝工艺制造氧化锆纳米纤维,并在该程序中使用聚乙烯吡咯烷酮(PVP)。 SEM,TGA,FT-IR和XRD用于研究电纺过程。在与比较相同的条件下对纯PVP进行静电纺丝。结果表明,纤维的平均直径为约80nm,表面光滑。 FT-IR光谱和TGA曲线证明热处理后PVP从纤维中去除。 -发现氧化锆的晶体结构在不同的煅烧温度下变化。 PVP,水和乙醇的双组分溶剂以及无机盐的使用对纤维的形态有积极的影响。

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