Reactivity of electrogenerated thiocyanogen in the thiocyanation of pyrazolo1,5-apyrimidines

Kokorekin Vladimir A.; Yaubasarova Rauza R.; Neverov Sergei V.Petrosyan Vladimir A.

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Reactivity of electrogenerated thiocyanogen in the thiocyanation of pyrazolo1,5-apyrimidines

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Selective thiocyanation (yield 70-90) at the 3-position of pyrazolo1,5-apyrimidines was performed with thiocyanogen electrochemically generated in situ from NH4SCN in MeCN on a Pt anode. For substrates with higher oxidation potential addition of Lewis acids was necessary.

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《Mendeleev Communications 》 |2016年第5期| 413-414| 共2页
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Kokorekin Vladimir A.; Yaubasarova Rauza R.; Neverov Sergei V.Petrosyan Vladimir A.;
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Russian Acad Sci, ND Zelinsky Inst Organ Chem, Moscow 119991, Russia;

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正文语种英语
中图分类化学 ;
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1. Pyrazolo(1,5-a)pyrimidines, triazolo(1,5-a)pyrimidines and their tricyclic derivatives as corticotropin-releasing factor 1 (CRF) receptor antagonists. [J] . Saito T, Obitsu T, Minamoto CSugiura TMatsumura NUeno SKishi AKatsumata SNakai HToda M Bioorganic and medicinal chemistry . 2011 ,第20期

机译：Pyrazolo(1,5-a)pyrimidines, triazolo(1,5-a)pyrimidines and their tricyclic derivatives as corticotropin-releasing factor 1 (CRF) receptor antagonists.
2. ChemInform Abstract: Reactivity of 7‐(2‐Dimethylaminovinyl)pyrazolo(1,5‐a)pyrimidines: Synthesis of Pyrazolo(1,5‐a)pyrido(3,4‐e)pyrimidine Derivatives as Potential Benzodiazepine Receptor Ligands. Part 1. [J] . F. BRUNI, S. SELLERI, A. COSTANZOG. GUERRINIM. L. CASILLI Chem Inform . 1995 ,第14期

机译：ChemInform Abstract: Reactivity of 7‐(2‐Dimethylaminovinyl)pyrazolo(1,5‐a)pyrimidines: Synthesis of Pyrazolo(1,5‐a)pyrido(3,4‐e)pyrimidine Derivatives as Potential Benzodiazepine Receptor Ligands. Part 1.
3. ChemInform Abstract: Reactivity of 7‐(2‐Dimethylaminovinyl)pyrazolo(1,5‐a)pyrimidines: Synthesis of Pyrazolo(1,5‐a)pyrido(3,4‐e)pyrimidine Derivatives as Potential Benzodiazepine Receptor Ligands. Part 2. [J] . F. BRUNI, S. SELLERI, A. COSTANZOG. GUERRINIM. L. CASILLIL. GIUSTI Chem Inform . 1995 ,第31期

机译：ChemInform Abstract: Reactivity of 7‐(2‐Dimethylaminovinyl)pyrazolo(1,5‐a)pyrimidines: Synthesis of Pyrazolo(1,5‐a)pyrido(3,4‐e)pyrimidine Derivatives as Potential Benzodiazepine Receptor Ligands. Part 2.
4. Discovery of 5-Amino-N-(1H-pyrazol-4-yl)pyrazolo1,5-apyrimidine-3-carboxamide Inhibitors of IRAK4 [O] . Jongwon Lim, Michael D. Altman, James Baker, 2015

机译：发现5-氨基-N-（1H-吡唑-4-基）Pyrazolo 1,5-A嘧啶-3-甲酰胺抑制剂的Irak4

Reactivity of electrogenerated thiocyanogen in the thiocyanation of pyrazolo1,5-apyrimidines

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