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Microwave-Assisted Synthesis of 3-Styrylchromones in Alkaline Ionic Liquid

机译:碱性离子液体中微波辅助合成3-苯乙烯基色酮

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摘要

A simple, highly efficient and environmentally benign method for the synthesis of 3-styrylchromones from 3-formylchromones and 4-nitrophenylacetic acid/4-nitrotolune in the presence of catalytic amount of basic ionic liquid 1-butyl-3-methylimidazolium hydroxide [(bmim)OH] carried out under the influence of microwave irradiation. This method gives remarkable advantages such as, short reaction times, simple work-up procedure and moderate to good yields. The ionic liquid was successfully reused for four cycles without significant loss of activity.
机译:一种简单,高效且环境友好的方法,在催化量的碱性离子液体氢氧化1-丁基-3-甲基咪唑鎓氢氧化物[[bmim )OH]在微波辐射的影响下进行。该方法具有显着的优点,例如反应时间短,后处理步骤简单以及产率中等至良好。离子液体成功重复使用了四个周期,而活性没有明显损失。

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