Characterization of Palladium(II) Azide and Crystal Structure of Bis(azido)bis(pyridine)palladium(II) and Tetramminepalladium Tetraazidopalladate(II)

Wolfgang Beck; Thomas M. Klapotke; Jorg Knizek; Heinrich Noth; Thomas Schutt

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Characterization of Palladium(II) Azide and Crystal Structure of Bis(azido)bis(pyridine)palladium(II) and Tetramminepalladium Tetraazidopalladate(II)

机译：叠氮化钯（II）的表征以及双（叠氮基）双（吡啶）钯（II）和四氨合钯四叠氮基钯（II）的晶体结构

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Palladium(II) azide (1) was synthesized by reaction of palladium nitrate and sodium azide. 1 was characterized by AAS, IR, and ~(14)N-NMR spectroscopy. Bis(azido)bis(pyridine)-palladium(II) (2) and tetramminepalladium tetraazido-palladate(II) (3) were synthesized by a high-yield reaction. Both were characterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy.

机译：通过硝酸钯与叠氮化钠的反应合成了叠氮化钯（II）（1）。通过AAS，IR和〜（14）N-NMR光谱表征图1。通过高产率反应合成了双（叠氮基）双（吡啶）-钯（II）（2）和四氨合钯四叠氮基-钯（II）（3）。两者均通过X射线结构分析，IR，拉曼和NMR光谱进行了表征。

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《European journal of inorganic chemistry》 |1999年第3期|共4页
作者
Wolfgang Beck; Thomas M. Klapotke; Jorg Knizek; Heinrich Noth; Thomas Schutt;
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正文语种 eng
中图分类无机化学;
关键词
palladium; azide; pyridine;

机译：钯;叠氮化物;吡啶;

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1. Characterization of Palladium(II) Azide and Crystal Structure of Bis(azido)bis(pyridine)palladium(II) and Tetramminepalladium Tetraazidopalladate(II) [J] . Wolfgang Beck, Thomas M. Klapotke, Jorg Knizek, European journal of inorganic chemistry . 1999,第3期

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Characterization of Palladium(II) Azide and Crystal Structure of Bis(azido)bis(pyridine)palladium(II) and Tetramminepalladium Tetraazidopalladate(II)

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