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Preparation and thermal stability of nickel nanowires via self-assembly process under magnetic field

机译:磁场下自组装法制备镍纳米线及其热稳定性

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Nickel nanowires were synthesized via a template-free method in an aqueous solution system combined with chemical reduction and magnetic field. The suitable concentration of Ni ions and reaction time were controlled in order to obtain nickel wires with uniform sizes. The products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, thermogravimetry and differential scanning calorimetry. The results showed that the Ni nanowires with large aspect ratio up to 200 had uniform size and morphology, about 200 nm. Especially, it is noteworthy that the samples were stable in air when the temperature was lower than 318 degrees C. The study would provide a facile method to prepare nickel nanowires with homogeneous diameter and high thermal stability, which could be used in catalysing CO2 hydrogenation.
机译:镍纳米线是通过无模板方法在水溶液体系中结合化学还原和磁场合成的。控制合适的镍离子浓度和反应时间,以获得尺寸均匀的镍丝。通过X射线衍射,扫描电子显微镜,透射电子显微镜,热重分析和差示扫描量热法对产物进行表征。结果表明,长宽比高达200的Ni纳米线具有均匀的尺寸和形态,约为200 nm。特别是,值得注意的是,当温度低于318摄氏度时,样品在空气中稳定。该研究将提供一种简便的方法来制备直径均一且热稳定性高的镍纳米线,该纳米线可用于催化CO2加氢。

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