Synthesis of 4-(1R,4R)-3-Oxo-p-menthan-2-ylidenemethylbenzoic Acid and Its Esters

T.G.Drushlyak; L.A.Kutulya; N.S.PivnenkoV.V.Vashchenko

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Synthesis of 4-(1R,4R)-3-Oxo-p-menthan-2-ylidenemethylbenzoic Acid and Its Esters

机译：4-（1R，4R）-3-氧代对薄荷烷-2-亚甲基苯甲酸及其酯类的合成

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Carbonylation of (E)-2-(4-halobenzylidene)-p-menthan-3-ones,catalyzed by PdCl_2(PPh_3)_2,gave a distereometric mixure of 4-(lR,4R)- and (1R,4S)-3-oxo-p-menthan-2-ylidenemethylbenzoic acids,whose reaction with phenols gave 1R,4R diastereomers of the corresponding esters.

机译：在PdCl_2（PPh_3）_2催化下，（E）-2-（4-卤代亚苄基）-对薄荷-3-酮羰基化反应，得到4-[（lR，4R）-和（1R，4S）-3-氧代对薄荷烷-2-亚甲基]苯甲酸的二立体混合物，其与酚类反应得到相应酯类的1R，4R非对映异构体。

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来源
《Russian Journal of General Chemistry》 |2005年第4期|622-627|共6页
作者
T.G.Drushlyak; L.A.Kutulya; N.S.PivnenkoV.V.Vashchenko;
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Institute of Monocrystals Scientific and Engineering Complex,National Academy of Sciences of Ukraine,Kharkov,Ukraine;

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正文语种英语
中图分类化学;
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Synthesis of 4-(1R,4R)-3-Oxo-p-menthan-2-ylidenemethylbenzoic Acid and Its Esters

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