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首页> 外文期刊>International Journal of Surface Science and Engineering >Nickel films prepared by electroless plating and arc discharge deposition methods on beech wood: physical and chemical properties
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Nickel films prepared by electroless plating and arc discharge deposition methods on beech wood: physical and chemical properties

机译:通过化学镀和电弧放电在山毛榉木上制备的镍膜:物理和化学性质

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摘要

Two methods, electroless plating and arc discharge deposition, were used to prepare nickel films on beech wood substrate. Coated films were characterised by scanning electron microscopy (SEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and the transverse electromagnetic (TEM) cell. The SEM results showed that the nickel covers the whole beech wood surface in all prepared films, with thickness varied from 0.7 mu m to 2.3 mu m. Using XRD, nickel crystallite sizes were measured to be 10 nm and 23 nm in electroless plating and arc discharge deposition methods, respectively. The XPS results demonstrated that the surface of the prepared films had a pure metallic nickel form without the presence of nickel oxide. Tests achieved with transverse electromagnetic cell (TEM cell) showed that an enhancement was detected in the measured electric field near the studied samples (at f = 1,500 MHz), which was found to be correlated with the quantity of nickel coated on beech wood surface and independent of the applied electromagnetic field level. The results of this study indicated that beech wood is a promising substrate for metal deposition in vacuum-plasma and chemical solution environment.
机译:化学镀和电弧放电沉积两种方法用于在山毛榉木基板上制备镍膜。通过扫描电子显微镜(SEM),X射线衍射(XRD),X射线光电子能谱(XPS)和横向电磁(TEM)池对涂膜进行表征。扫描电镜结果表明,镍覆盖了所有制备好的薄膜的整个榉木表面,厚度范围为0.7微米至2.3微米。使用XRD,在化学镀和电弧放电沉积方法中测得的镍微晶尺寸分别为10 nm和23 nm。 XPS结果表明,所制备的膜的表面具有纯金属镍形式,而没有氧化镍的存在。用横向电磁电池(TEM电池)进行的测试表明,在所研究样品附近(在f = 1,500 MHz处)测得的电场中检测到增强,这与山毛榉木表面镍涂层的镍含量有关。与施加的电磁场水平无关。这项研究的结果表明,榉木是在真空等离子体和化学溶液环境中用于金属沉积的有前途的基质。

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