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APPLICATION OF PIXE TO DETERMINATION OF ELEMENTS IN THE PLACENTA, MATERNAL BLOOD AND CORD BLOOD

机译:像素法在胎盘,母血和脐血中元素的测定中的应用

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摘要

PIXE technique was applied to the measurement of elements in the placenta, maternal blood and cord blood of human. The elements determined in these samples include Cl, K, Ca, Fe, Cu and Zn. The values obtained by PtXE were compared with those by ICP-AES to test the accuracy of the method. In placental samples, the mean values of K, Fe, Cu and Zn concentrations obtained by the two methods agree, while Ca concentration is lower in PIXE analysis. The values from PIXE, however, show larger variations resulting from inhomogeneity of the placental samples composed of various tissues different in hislological liinctions. In the analysis of blood samples, the results of the two methods agree for Cl. K. Ca. Fe, Cu and Zn. although the standard deviations tend to be larger in PIXE. These results indicate that PIXE is a useful method for the determination of elements in placental and blood samples, although the preparation to homogenize sample is necessary to obtain accurate results.
机译:PIXE技术用于人体胎盘,母血和脐带血中元素的测定。这些样品中确定的元素包括Cl,K,Ca,Fe,Cu和Zn。将PtXE所得的值与ICP-AES所得的值进行比较,以检验该方法的准确性。在胎盘样品中,通过两种方法获得的K,Fe,Cu和Zn浓度平均值一致,而PIXE分析中的Ca浓度较低。但是,PIXE的值显示出较大的变化,这是由组织学连接不同的各种组织组成的胎盘样品的不均匀性引起的。在血样分析中,两种方法的结果均符合Cl。钙铁,铜和锌。尽管PIXE中的标准偏差往往更大。这些结果表明,PIXE是测定胎盘和血液样品中元素的有用方法,尽管必须进行均质化样品的制备才能获得准确的结果。

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