Unexpected formation of 1,4-diphenylbutylphosphinic acid from 1,4-diphenylbuta-1,3-diene and elemental phosphorus via the Trofimov-Gusarova reaction

Artemev Alexander V.; Sutyrina Anastasiya O.; Matveeva Elena A.Albanov Alexander I.Klyba Lyudmila V.

首页> 外文期刊>Mendeleev Communications >Unexpected formation of 1,4-diphenylbutylphosphinic acid from 1,4-diphenylbuta-1,3-diene and elemental phosphorus via the Trofimov-Gusarova reaction

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Unexpected formation of 1,4-diphenylbutylphosphinic acid from 1,4-diphenylbuta-1,3-diene and elemental phosphorus via the Trofimov-Gusarova reaction

机译：1,4-二苯基丁基-1,3-二烯和元素磷通过Trofimov-Gusarova反应意外形成1,4-二苯基丁基次膦酸

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trans,trans-1,4-Diphenylbuta-1,3-diene reacts with elemental (red) phosphorus in the superbasic KOH/DMSO (H2O) system (120 degrees C, 3 h) to give, after acidic work-up, 1,4-di-phenylbutylphosphinic acid in 48 yield.

机译：反式，反式-1,4-二苯基丁-1,3-二烯与超碱性KOH/DMSO（H2O）体系（120°C，3小时）中的元素（红）磷反应，经过酸性处理后，得到1,4-二苯基丁基膦酸，收率为48%。

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来源
《Mendeleev Communications》 |2017年第2期|137-138|共2页
作者
Artemev Alexander V.; Sutyrina Anastasiya O.; Matveeva Elena A.Albanov Alexander I.Klyba Lyudmila V.;
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Russian Acad Sci, Siberian Branch, AE Favorsky Irkutsk Inst Chem, Irkutsk 664033, Russia;

Russian Acad Sci, Siberian Branch, AV Nikolaev Inst Inorgan Chem, Novosibirsk 630090, Russia;

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中图分类化学;
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Unexpected formation of 1,4-diphenylbutylphosphinic acid from 1,4-diphenylbuta-1,3-diene and elemental phosphorus via the Trofimov-Gusarova reaction

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