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首页> 外文期刊>International journal of mass spectrometry >Simplified injector flanges for the selected ion flow tube
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Simplified injector flanges for the selected ion flow tube

机译:所选离子流管的简化进样器法兰

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摘要

Dual hole-pattern injector flanges (Venturi inlets) for a selected ion flow tube have been fabricated and tested in order to identify an optimum balance of efficient operational characteristics and simplicity of fabrication, along with reproducible assembly. The diagnostic measurements for each configuration addressed: (a) ability to maintain pressure differences between ion selection and ion reaction regions; (b) ability to inject sufficient ions to carry out ion/molecule reaction studies; and (c) ability to not introduce turbulence in the reaction region of the flow tube. In addition, the sensitivity of these issues to different total gas flow and to partitioning of total flow between inner and outer injectors is considered. All hole-pattern injector configurations ever tried worked without requiring any adjusting. Importantly, extensive kinetic measurements of one ion/molecule reaction for many configurations, gas loads, and partitions, indicate turbulence in the reaction region is never a problem for these injectors. An injector flange with a small total helium inlet area via 12 holes, in a planar surface, with the ion orifice slightly downstream of the helium inlet plane, has provided the best experimental data.
机译:已制造并测试了用于选定离子流管的双孔型进样器法兰(文丘里管入口),以便确定有效运行特性和制造简便性以及可重复组装之间的最佳平衡。针对每种配置的诊断测量结果涉及:(a)保持离子选择区与离子反应区之间压力差的能力; (b)注入足够的离子以进行离子/分子反应研究的能力; (c)在流量管的反应区域不引入湍流的能力。另外,考虑到这些问题对不同的总气体流量以及内部和外部喷射器之间的总流量分配的敏感性。曾经尝试使用所有孔型喷油器配置,而无需进行任何调整。重要的是,对于许多构型,气体负载和隔板,对一个离子/分子反应进行的广泛动力学测量表明,对于这些注射器,反应区域中的湍流从来都不是问题。在平坦表面上通过12个孔具有较小的总氦气入口面积的进样器法兰,离子孔位于氦气入口平面的下游,提供了最佳的实验数据。

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