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Assessment of residue melamine in dairy products exhibited in Zanjan market, Iran by high-performance liquid chromatography method

机译:高效液相色谱法评估伊朗赞詹市场上展出的乳制品中的残留三聚氰胺

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摘要

An increasing number of infants are being made sick by dairy products contaminated with melamine. As a result, many countries have adopted additional requirements for milk-based food products. The scope of the present study was to assess amounts of melamine in some dairy products from Zanjan market, Iran. Amounts of melamine in samples of milk, yoghurt, infant formula, coffee mate and cheese were determined in five different brands by the high-performance liquid chromatography with ultraviolet detector system. In total, 225 samples were determined (five products x five brands x three samples x three repeated measurements). Amounts of melamine in samples (in mu g/g) were determined in the range of 0.20-0.26 for milk, 0.57-0.99 for yoghurt, 0.35-3.40 for infant formula, 0.09-1.23 for coffee mate and 0.30-2.50 for cheese, and the mean values of melamine in products were evaluated as 0.24, 0.76, 1.38, 0.56 and 1.16, respectively. The minimum and maximum values for amounts of melamine were recorded in milk and infant formula, respectively. Comparison of test results with the standards set by the European Union and the US Food and Drug Administration for maximum residue-level values for dairy products contaminated with melamine showed that levels determined by tests had higher health risks than the regulations allowed. Iran has not yet adopted regulations to control levels of melamine in food products. The results show that maximum residue-level values need to be determined for melamine in Iranian dairy products, and foods should be monitored daily for levels of melamine contamination.
机译:被三聚氰胺污染的乳制品使越来越多的婴儿患病。结果,许多国家对基于牛奶的食品采取了额外的要求。本研究的范围是评估伊朗Zanjan市场的某些乳制品中的三聚氰胺含量。通过具有紫外检测器系统的高效液相色谱法,在五个不同品牌中测定了牛奶,酸奶,婴儿配方奶粉,咖啡伴侣和奶酪中三聚氰胺的含量。总共确定了225个样本(五个产品x五个品牌x三个样本x三个重复测量)。样品中三聚氰胺的含量(以微克/克计)在牛奶中为0.20-0.26,酸奶中为0.57-0.99,婴儿配方中为0.35-3.40,咖啡伴侣为0.09-1.23,奶酪为0.30-2.50。产品中三聚氰胺的平均值分别为0.24、0.76、1.38、0.56和1.16。三聚氰胺含量的最小值和最大值分别记录在牛奶和婴儿配方奶粉中。将测试结果与欧盟和美国食品和药物管理局设定的关于三聚氰胺污染的乳制品的最大残留水平值进行比较,结果表明,通过测试确定的水平具有比规定允许的更高的健康风险。伊朗尚未通过法规来控制食品中三聚氰胺的含量。结果表明,需要确定伊朗乳制品中三聚氰胺的最大残留水平,并且应每天监控食品中三聚氰胺的污染水平。

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