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Quantitative Measurement of Propellant Stabilizers with tlc and liquid‐crystalline method of visualization

机译:使用TLC和液晶可视化方法对推进剂稳定剂进行定量测量

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AbstractBasic compounds of propellants, nitrate esters decompose forming nitrogen oxides as the catalytic products. To inhibit further decomposition, stabilizer reacts with nitrogen oxides, and finally non‐catalytic products are formed, so autocatalytic decomposition is minimized. In this way, chemical stability of propellant increases, but the content of stabilizer decreases.In this paper, the possibility of quantitative analysis of the weight loss of propellant stabilizer using the TLC method and the liquid crystal method of visualization is presented. The advantages of solid phase extraction (SPE) application in such analysis are also show
机译:摘要推进剂的基本化合物硝酸酯分解生成氮氧化物作为催化产物。为了抑制进一步分解,稳定剂与氮氧化物反应,最终形成非催化产物,从而最大限度地减少自催化分解。这样,推进剂的化学稳定性增加,但稳定剂的含量降低。本文提出了利用TLC法和液晶法对推进剂稳定剂失重进行定量分析的可能性。固相萃取(SPE)在此类分析中的应用优势也得到了体现

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