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Spectral and surface analysis of heated micro-column arrays fabricated by laser-assisted surface modification

机译:激光辅助表面修饰制备的加热微柱阵列的光谱和表面分析

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摘要

Micro-column array (MCA) structures fabricated by laser ablation of tungsten, tantalum, molybdenum, titanium, alloy 321, and Hastelloy276~(TM) foils have been tested as possible candidates for wide-spectrum optical calibration sources and characterized. The surface of one side of the foil was structured to obtain periodically distributed micro-cones and micro-cavities. The spectral characteristics from samples of selected materials were measured at temperatures in the range from 500 to 1360℃ achieved by resistive heating of the foil samples in vacuum. Such characteristics measured from the MCA-structured surfaces of all foils show a significant enhancement towards the ideal blackbody and blackbody simulator characteristics compared to the non-structured surfaces. Surface modification of the MCA-structured samples was investigated using optical microscopy, scanning electron microscopy, and X-ray photoemission spectroscopy. Results obtained from tantalum-based samples indicated that they may be suitable for applications in blackbody-like emission devices.
机译:已经测试了通过激光烧蚀钨,钽,钼,钛,合金321和Hastelloy276〜(TM)箔制成的微柱阵列(MCA)结构,并已将其用作广谱光学校准源的候选材料并进行了表征。箔的一侧的表面被结构化以获得周期性分布的微锥和微腔。通过在真空中对箔样品进行电阻加热,在500至1360℃的温度范围内测量所选材料样品的光谱特性。与非结构化表面相比,从所有箔的MCA结构化表面测得的此类特性均朝着理想的黑体和黑体模拟器特性显着增强。使用光学显微镜,扫描电子显微镜和X射线光电子能谱研究了MCA结构化样品的表面改性。从钽基样品获得的结果表明,它们可能适用于类黑体发射设备。

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