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Comprehensive utilization of the hydrolyzed productions from rice hull.

机译:稻壳水解产物的综合利用。

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The study based on pretreatment, hydrolyzation and separation processes with the raw material rice hull, provides a comprehensive utilization of the hydrolyzed productions, such as glucose (C6H12O6) from cellulose, silica (SiO2), and byproduct crystalline sodium sulfate (Na2SO4.10H2O). The optimum hydrolysis conditions are as follows: the concentration of H2SO4 is 72% (wt.%), the temperature is 50 degrees C, the ratio of H2SO4 solution volume (mL) to the rice hull mass (g) is 10:1 and the time is 5 min, the glucose yield rate reaches 45.6% (wt.%). The concentration of glucose solution could be 0.1 g/mL after neutralization measured by ultraviolet spectrophotometer (UV-VIS). Silica powder was below 50 nm characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The main byproduct crystalline sodium sulfate was featured by XRD and photographs.
机译:基于原料稻壳的预处理,水解和分离过程的研究提供了水解产物的综合利用,例如葡萄糖(C 6 H 12 O <纤维素,二氧化硅(SiO 2 )和副产物结晶硫酸钠(Na 2 SO 4 .10H)中的sub> 6 2 O)。最佳水解条件如下:H 2 SO 4 的浓度为72%(重量%),温度为50℃,H < sub> 2 SO 4 溶液体积(mL)与稻壳质量(g)的比例为10:1,时间为5分钟,葡萄糖的得率达到45.6%(wt。 %)。通过紫外分光光度计(UV-VIS)测量中和后葡萄糖溶液的浓度可以为0.1g / mL。二氧化硅粉末在50nm以下,通过X射线衍射(XRD)和扫描电子显微镜(SEM)表征。 X射线衍射和照片表征了主要副产物结晶硫酸钠。

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