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Effects of microwave irradiation on the basic properties of woodceramics made from carbonized tobacco stems impregnated with phenolic resin

机译:微波辐射对浸渗酚醛树脂的碳化烟梗制得的木陶瓷基本性能的影响

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摘要

A series of woodceramics derived from carbonized tobacco stems and phenolic resin composite heated by microwave irradiation was prepared and effects of microwave irradiation time, power and mass fraction of phenolic resin in woodceramics on the mass loss ratio, volume shrinkage ratio, apparent density, open porosity and volume electrical resistivity were investigated systematically. The pyrolysis behaviours of tobacco stems, phenolic resin and carbonized tobacco stems/phenolic resin composite were also evaluated using thermogravimetry. The experimental results showed that the mass loss ratio, volume shrinkage ratio and apparent density increased, while the volume electrical resistivity and open porosity decreased with increasing microwave irradiation time. The apparent density increased, while the mass loss ratio, volume shrinkage ratio, volume electrical resistivity and open porosity decreased with an increase in the mass fraction of phenolic resin. The mass loss ratio, volume shrinkage ratio and open porosity increased, while apparent density and volume electrical resistivity decreased with an increase in the microwave power. Microstructures of woodceramics obtained at various microwave irradiation time were characterized by scanning electron microscopy (SEM) technique, which confirmed the results of pyrolysis analyses of samples and effects of microwave irradiation on basic properties of woodceramics prepared.
机译:制备了一系列由炭化烟梗和酚醛树脂复合材料经微波辐射加热的木陶瓷,微波辐射时间,功率和酚醛树脂在木陶瓷中的质量分数对质量损失率,体积收缩率,表观密度,开孔率的影响对体积电阻率进行了系统的研究。还使用热重分析法评估了烟梗,酚醛树脂和碳化烟梗/酚醛树脂复合材料的热解行为。实验结果表明,随着微波辐照时间的增加,质量损失率,体积收缩率和表观密度增加,而体积电阻率和开孔率降低。表观密度增加,而质量损失率,体积收缩率,体积电阻率和开孔率随酚醛树脂质量分数的增加而降低。随着微波功率的增加,质量损失率,体积收缩率和开孔率增加,而表观密度和体积电阻率降低。通过扫描电子显微镜(SEM)表征了在各种微波辐照时间下获得的木陶瓷的微观结构,证实了样品的热解分析结果以及微波辐照对制备的木陶瓷基本性能的影响。

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