Synthesis of some novel 3,5-diarylpyrazole derivatives of dibenzo-18-crown-6-ether

S D Jagadale; A G Mulik; D R Chandam

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Synthesis of some novel 3,5-diarylpyrazole derivatives of dibenzo-18-crown-6-ether

机译：新型二苯并-18-冠-6-醚的3,5-二芳基吡唑衍生物的合成

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Novel pyrazole derivatives of dizenzo-18-crown-6-elher arc obtained via three step protocol involving acylation of dibenzo-18-crown-6 1 followed by the condensation with various aromatic aldehydes to form the corresponding chalcones 3, which on helerocyclisation with hydrazine hydrate give the target molecule 4. These new molecules have been characterized on the basis of IR, ~1H NMR, ~(13)C NMR and elemental analysis.

机译：通过三步方案获得的二氮杂-18-冠-6-elher的新型吡唑衍生物，包括将二苯并-18-18-冠-6 1酰化，然后与各种芳族醛缩合形成相应的查耳酮3，将其与肼一起进行环化水合物可得到目标分子4。这些新分子已根据IR，〜1H NMR，〜（13）C NMR和元素分析进行了表征。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2013年第10期|共5页
作者
S D Jagadale; A G Mulik; D R Chandam;
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正文语种 eng
中图分类化学;
关键词
Dibenzo-18-crown-6; acylation; chalcone; iodine; pyrazole;

机译：二苯并18-冠-6;酰化;查尔酮;碘;吡唑;

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1. Synthesis of some novel 3,5-diarylpyrazole derivatives of dibenzo-18-crown-6-ether [J] . S D Jagadale, A G Mulik, D R Chandam Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2013,第10期

机译：新型二苯并-18-冠-6-醚的3,5-二芳基吡唑衍生物的合成
2. 3,5-Diarylpyrazole Derivatives Obtained by Ammonolysis of the Total Flavonoids from Chrysanthemum indicum Extract Show Potential for the Treatment of Alzheimer's Disease [J] . Wu Taizong, Jiang Cheng, Wang Ling, Journal of natural products . 2015,第7期

机译：菊苣提取物中总黄酮氨解获得的3,5-二芳基吡唑衍生物显示出治疗阿尔茨海默氏病的潜力
3. Regioselective one-pot synthesis of 3,5-diarylpyrazoles [J] . P D Lokhande, B Y Waghamare, S S Sakate Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2005,第11期

机译：区域选择性一锅合成3,5-二芳基吡唑
4. Combining performance with thermal stability: Synthesis and characterization of 5-(3,5-dinitro-1H-pyrazol-4-yl)-1H-tetrazole and its energetic derivatives [C] . Maximilian Benz, Thomas M. Klapoetke, Joerg Stierstorfer Seminar on new trends in research of energetic materials . 2020

机译：性能兼具热稳定性：5-（3,5-二硝基-1H-吡唑-4-基）-1H-四唑及其高能衍生物的合成与表征
5. Synthesis and photochemistry of 3,5-dialkyl-3,5-dihydro-3,5-diphenyl-4H-pyrazol-4-ones. [D] . Moiseev, Andrey G. 2006

机译：3，5-二烷基-3，5-二氢-3，5-二苯基-4H-吡唑-4-酮的合成和光化学。
6. 3D QSAR studies pharmacophore modeling and virtual screening of diarylpyrazole–benzenesulfonamide derivatives as a template to obtain new inhibitors using human carbonic anhydrase II as a model protein [O] . Yeganeh Entezari Heravi, Hassan Sereshti, Ali Akbar Saboury, 2017

机译：3D QSAR研究药效团建模和以人碳酸酐酶II为模型蛋白的二芳基吡唑-苯磺酰胺衍生物作为模板的虚拟筛选以获得新的抑制剂
7. Synthesis and Herbicidal Activity of 1,5-Diarylpyrazole Derivatives. [O] . Noriaki KUDO, Satoru FURUTA, Misa TANIGUCHI, 1999

机译：1,5-二芳基吡唑衍生物的合成和除草活性。
8. Theoretical Prediction of the Heats of Formation, Densities and Relative Sensitivities, and/or Synthetic Approaches Toward the Synthesis of High Energy Dense Materials (HEDMs): 3,5-Dinitro-1,3,5-Oxadiazinane, Bis-Adjacent RDX, Bis-Adjacent HMX, 4,4',6,6'-Tetranitro-1,1'-Bis(N-oxide)-5,5',6,6'-4H,4'H-5,5'-Bisimidazo Oxadiazole, and the Open-Cage Derivative of CL-20. [R] . Byrd, E. F., Sabatini, J. J. 2015

机译：形成热，密度和相对灵敏度的理论预测，和/或合成高能量密集材料（HEDms）的合成方法：3,5-二硝基-1,3,5-恶二唑烷，双相邻RDX，Bis - 相邻的HmX，4,4'，6,6'-四硝基-1,1'-双（N-氧化物）-5,5'，6,6'-4H，4'H-5,5'-双咪唑恶二唑和CL-20的开笼衍生物。

Synthesis of some novel 3,5-diarylpyrazole derivatives of dibenzo-18-crown-6-ether

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