Electrochemical Synthesis of Niobium Compounds in Anodic Dissolution of Ferroniobium in Methanol

摘要

Anodic dissolution of ferroniobium in anhydrous methanol in the presence of sodium methylate was studied. The possibility of recovering pure hexamethoxyniobate from the electrolyzate and its conversion into niobium methylate with an iron content not exceeding 0.01 was analyzed.