A simple and efficient PTT-mediated synthesis of a-azidoketones in [bmim][BF4] ionic liquid

Anil Kumar; Israr Ahmed; M Sudershan Rao

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A simple and efficient PTT-mediated synthesis of a-azidoketones in [bmim][BF4] ionic liquid

机译：[bmim] [BF4]离子液体中简单高效的PTT介导的a-叠氮酮的合成

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摘要

A simple and efficient one-pot method has been described for the direct synthesis of a-azidoketones from various ketones possessing a-hydrogen by reaction with phenyltrimethylammo-nium tribromide (PTT) and subsequent treatment with NaN3 in ionic liquid. The procedure gives high yield and the ionic liquid can be reused.

机译：已经描述了一种简单有效的一锅法，该方法可通过与苯基三甲基铵三溴化铵（PTT）反应并随后在离子液体中用NaN3处理，从具有a-氢的各种酮中直接合成α-叠氮酮。该程序产率高，并且离子液体可以重复使用。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2009年第4期|共6页
作者
Anil Kumar; Israr Ahmed; M Sudershan Rao;
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正文语种 eng
中图分类化学;
关键词
Phenyltrimethylammonium tribromide (PTT); α-azidoketones; ionic liquid;

机译：苯基三甲基三溴化铵（PTT）;α-叠氮酮;离子液体;

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1. A simple and efficient PTT-mediated synthesis of a-azidoketones in [bmim][BF4] ionic liquid [J] . Anil Kumar, Israr Ahmed, M Sudershan Rao Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2009,第4期

机译：[bmim] [BF4]离子液体中简单高效的PTT介导的a-叠氮酮的合成
2. LiBF4 integrated into [BMIm]BF4: an ionic-liquid metal composite and homogeneous catalyst for efficient synthesis of pyran-annulated heterocycles [J] . Kurosh Rad-Moghadam, Alireza Taghizadeh Valadi, Arefeh Alipour Applied Organometallic Chemistry . 2014,第3期

机译：LiBF4集成到[BMIm] BF4中：离子液体金属复合物和均相催化剂，可有效合成吡喃环化的杂环
3. Ionic Liquid [bmim]BF4 as an Efficient and Recyclable Reaction Medium for the Synthesis of O-Acetyl Cyanohydrin via One-Pot Condensation of Aldehyde, TMSCN, and Ac2O [J] . Shen ZL, Ji SJ Synthetic Communications . 2009,第4a6期

机译：离子液体[bmim] BF4作为通过醛，TMCSN和Ac2O的一锅缩合反应合成O-乙酰基氰醇的高效可循环反应介质
4. Synthesis of Acidic Ionic Liquids Functionalized Ordered Mesoporous Polymer for Efficient, Green and Low Cost Production of Biodiesel from waste brown grease [C] . Iman Noshadi, Baishali Kanjilal, Steven Suib National Meeting Exhibition . 2013

机译：酸性离子液体的合成官能化有序的介孔聚合物，从废棕色油脂中有效，绿色和低成本生产生物柴油
5. Effect of the [BMIM][BF4] as a mobile phase additives on the adsorption behavior of tryptophan by reversed-phase high performance liquid chromatography. [D] . Vegesna, Vijaya Sree. 2010

机译：反相高效液相色谱法[BMIM] [BF4]作为流动相添加剂对色氨酸的吸附行为的影响。
6. Rapid and Efficient Separation of Decursin and Decursinol Angelate from Angelica gigas Nakai using Ionic Liquid (BMIm)BF4 Combined with Crystallization [O] . Alice Nguvoko Kiyonga, Ji-Hun An, Ki Yong Lee, 2019

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7. [Bmim]BF4 ionic liquid: An efficient reaction medium for the one-pot multi-component synthesis of 2-amino-4,6-diphenylpyridine-3-carbonitrile derivatives [O] . S. Sheik Mansoor, K. Aswin, K. Logaiya, 2016

机译：[Bmim] BF4离子液体：一锅多组分合成2-氨基-4,6-二苯基吡啶-3-甲腈衍生物的有效反应介质

A simple and efficient PTT-mediated synthesis of a-azidoketones in [bmim][BF4] ionic liquid

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