AlCl_3 mediated three component cyclocondensation for the synthesis of 5-unsubstituted 3,4-dihydropyrimidi%2(1H)-ones

Anil Saini; Sanjay Kumar; Jagir S Sandhu

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AlCl_3 mediated three component cyclocondensation for the synthesis of 5-unsubstituted 3,4-dihydropyrimidi%2(1H)-ones

机译：AlCl_3介导的三组分环缩合反应，用于合成5-未取代的3,4-二氢嘧啶％2（1H）-ones

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摘要

5-Unsubstituted-3,4-dihydropyrimidin-2(1H)-ones have been synthesized in excellent yields in aluminium trichloride mediated three -component- cyclocondensation of aldehyde,urea and enolisable ketones.

机译：在三氯化铝介导的醛，脲和可缩合酮的三组分环缩合反应中，以优异的产率合成了5-未取代的3,4-二氢嘧啶-2（1H）-酮。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2006年第3期|共5页
作者
Anil Saini; Sanjay Kumar; Jagir S Sandhu;
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正文语种 eng
中图分类化学;
关键词
Aluminium trichloride; potassium iodide; enolisalable keldne; addehyde; urea; 5-unsubstituted-3; 4-dihydropyrimidin-2(1H)-ones;

机译：三氯化铝;碘化钾;烯醇化钾;醛;脲;5-未取代-3;4-二氢嘧啶-2（1H）-;

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1. AlCl_3 mediated three component cyclocondensation for the synthesis of 5-unsubstituted 3,4-dihydropyrimidi%2(1H)-ones [J] . Anil Saini, Sanjay Kumar, Jagir S Sandhu Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2006,第3期

机译：AlCl_3介导的三组分环缩合反应，用于合成5-未取代的3,4-二氢嘧啶％2（1H）-ones
2. Novel Biginelli-like three-component cyclocondensation reaction:efficient synthesis of 5-unsubstituted 3,4-dihydropyrimidin-2(1H)-ones [J] . Zong-Ting Wang, Li-Wen Xu, Chun-Gu Xia, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2004,第42期

机译：新型Biginelli样三组分环缩合反应：5-未取代的3,4-二氢嘧啶-2（1H）-ones的高效合成
3. Iodotrimethylsilane-Accelerated One-Pot Synthesis of 5-Unsubstituted 3,4-Dihydropyrimidin-2(1H)-ones:A Novel Procedure for the Biginelli-Like Cyclocondensation Reaction at Room Temperature) [J] . Gowravarani Sabitha, Kusuma B.Reddy, Rangavajjula Srinivas, Helvetica chimica acta . 2005,第11期

机译：碘代三甲基硅烷促进一锅法合成5-未取代的3,4-二氢嘧啶-2（1H）-ones：室温下类似于Biginelli的环缩反应的新方法）
4. Synthesis and Characterization of 3,4-Dihydropyrimidine-2(1H)-One (DHPM) Derivatives Doped Acrylic Polymers for Thin Film Coatings [C] . Balaji Walekar, Ramaraje Mane, Sameer Nadaf International Conference on Polymer Processing and Characterization . 2016

机译：3,4-二氢嘧啶-2（1H） - 酮（DHPM）衍生物掺杂薄膜涂料的合成及表征掺杂丙烯酸聚合物
5. Electrochemical synthesis and characterization of polymers from bis(3,4-ethylenedioxythiophene)-thiophenes (BEDOT-Ts) and bis(3,4-ethylenedioxythiophene)-benzenes (BEDOT-Bs) as optoelectronic materials. [D] . Eaiprasertsak, Kalya. 2008

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6. An Efficient One-Pot Green Protocol for the Synthesis of 5-Unsubstituted 34-Dihydropyrimidin-2(1H)-Ones Using Recyclable Amberlyst 15 DRY as a Heterogeneous Catalyst via Three-Component Biginelli-Like Reaction [O] . Srinivasa Rao Jetti, Divya Verma, Shubha Jain 2012

机译：一种高效的一锅绿色协议使用可回收的Amberlyst 15 DRY作为三元类似Biginelli相似反应的多相催化剂用于合成5-Un取代的34-Dihydropyrimidin-2（1H）-
7. An Efficient One-Pot Green Protocol for the Synthesis of 5-Unsubstituted 3,4-Dihydropyrimidin-2(1H)-Ones Using Recyclable Amberlyst 15 DRY as a Heterogeneous Catalyst via Three-Component Biginelli-Like Reaction [O] . Srinivasa Rao Jetti, Divya Verma, Shubha Jain 2012

机译：一种有效的单盆绿的绿色方案，用于合成5-未取代的3,4-二氢嘧啶-2（1H） - 通过三组分的Biginelli反应作为非均相催化剂作为非均相催化剂的5-未取代的3,4-二氢嘧啶-2（1H）-ONE

AlCl_3 mediated three component cyclocondensation for the synthesis of 5-unsubstituted 3,4-dihydropyrimidi%2(1H)-ones

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