A rapid method for oxidative deprotection of trimethylsily ether with wet alumina supported Dess-Martin perodinane in solventless system under microwave irradiation

S Hossein Abdi Oskooie; majid M Heravi; Noohshin Sarmad; Akbar Saednia; Mitra Ghassemzadeh

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A rapid method for oxidative deprotection of trimethylsily ether with wet alumina supported Dess-Martin perodinane in solventless system under microwave irradiation

机译：微波辐射下无溶剂体系中湿式氧化铝负载的Dess-Martin过碘烷氧化三甲基甲醚的快速方法

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摘要

Primary and secondary trimethylsilyl ethers have been rapidly coverted to the corresponding carbonyl compounds using Dess-Martin perodinance supported on to wet alumina in a solventless system under microwave irradiation.

机译：使用在微波辐射下在无溶剂体系中负载在湿氧化铝上的Dess-Martin介导剂，伯和仲三甲基甲硅烷基醚已迅速被掩盖在相应的羰基化合物上。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2003年第11期|共2页
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S Hossein Abdi Oskooie; majid M Heravi; Noohshin Sarmad; Akbar Saednia; Mitra Ghassemzadeh;
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1. A rapid method for oxidative deprotection of trimethylsily ether with wet alumina supported Dess-Martin perodinane in solventless system under microwave irradiation [J] . S Hossein Abdi Oskooie, majid M Heravi, Noohshin Sarmad, Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2003,第11期

机译：微波辐射下无溶剂体系中湿式氧化铝负载的Dess-Martin过碘烷氧化三甲基甲醚的快速方法
2. Wet Alumina Supported Chromium(VI) Oxide: A Mild, Efficient and Inexpensive Reagent for Oxidative Deprotection of Trimethylsilyl and Tetrahydropyranyl Ethers in a Solventless System [J] . Majiid M. Heravi, Dariush Ajami, Mitra Ghassemzadeh Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 1999,第3期

机译：湿氧化铝负载的氧化铬（VI）：一种无溶剂系统中三甲基甲硅烷基和四氢吡喃基醚氧化脱保护的温和，高效且廉价的试剂
3. Direct oxidative deprotection of trimethylsilyl ethers with cerium ammonium nitrate supported onto HZSM-5 zeolite under microwave irradiation in solventless system [J] . Hossein A Oskooie, Somaih Solemani Amiri, Majid M Heravi, Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2006,第3期

机译：无溶剂体系中微波辐射下HZSM-5分子筛上负载硝酸铈铵的三甲基甲硅烷基醚的直接氧化脱保护
4. PREPARATION OF METAL OXIDES BY POLYOL METHOD UNDER MICROWAVE IRRADIATION [C] . Tetsushi Yamamoto, Yuji Wada, Shozo Yanagida World congress on microwave and radio frequency applications . 2003

机译：微波辐射下多元醇法制备金属氧化物
5. THE DEVELOPMENT OF A NEW PRETREATMENT METHOD (RAPID STEAM HYDROLYSIS) AND THE COMPARISON OF RAPID STEAMING, STEAM EXPLOSION, AUTOHYDROLYSIS, AND WET OXIDATION AS PRETREATMENT PROCESSES FOR BIOMASS CONVERSION OF SOUTHERN HARDWOODS. [D] . BIERMANN, CHRISTOPHER JAMES. 1983

机译：新型预处理方法（快速蒸汽水解）的开发以及快速蒸煮，蒸汽爆炸，自水解和湿式氧化作为南方硬木生物转化的预处理方法的比较。
6. Microwave Assisted Synthesis Part 1: Rapid Solventless Synthesis of 3-Substituted Coumarins and Benzocoumarins by Microwave Irradiation of the Corresponding Enaminones [O] . Khadijah M. Al-Zaydi 2003

机译：微波辅助合成第1部分：通过相应的烯胺酮的微波辐射快速合成3-取代的香豆素和苯并香豆素
7. Microwave Assisted Synthesis, Part 1: Rapid Solventless Synthesis of 3Substituted Coumarins and Benzocoumarins by Microwave Irradiation of Corresponding Enaminones [O] . Khadijah M. Al-zaydi 2014

机译：微波辅助合成，第1部分：微波辐射相应的烯胺酮快速无溶剂合成3取代香豆素和苯并香豆素
8. An Improved Microwave Digestion System for Rapid Wet Ashing of Biological Fluids and Tissues. [R] . Anand, V. D., Lancaster, M. C., Troxler, R. G., 1977

机译：一种改进的微波消解系统用于生物流体和组织的快速湿法灰化。

A rapid method for oxidative deprotection of trimethylsily ether with wet alumina supported Dess-Martin perodinane in solventless system under microwave irradiation

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