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Microstructural and topographical characterization of different surface treatments of a surgical titanium alloy for dental implants

机译:牙科植入物用外科钛合金不同表面处理的微观结构和形貌特征

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摘要

OBJECTIVE: To perform a topographical characterization of a titanium alloy subjected to different surface treatments using roughness evaluation, scanning electron microscopy, and atomic force microscopy. Materials and methods: For each group, 6 discs of a titanium alloy had their surfaces modified by 4 treatments. All surfaces were blasted with Al2O3, cleaned, and the specimens were divided into 4 groups: G1, immersion in a standardized acid solution (SAS) (control group); G2, immersion in acetone, followed by immersion in SAS; G3, immersion in acetone, followed by immersion in SAS, followed by immersion in nitric acid; G4, immersion in acetone, followed by immersion in SAS, followed by immersion in sulfuric acid. Roughness parameters were determined with a roughness tester, and data were statistically analyzed using analysis of variance and Tukey tests (α = 5%). RESULTS: Regarding the roughness parameters, no significant differences were found. Scanning electron microscopy and atomic force microscopy showed irregular surfaces with the presence of particles uniformly deposited on the surfaces. CONCLUSION: A similar roughness pattern was created for all the groups. The images and topographic profiles indicated that all the groups showed high levels of roughness.
机译:目的:使用粗糙度评估,扫描电子显微镜和原子力显微镜对经过不同表面处理的钛合金进行形貌表征。材料和方法:对于每组,通过4次处理对6个钛合金圆盘进行表面改性。所有表面均用Al2O3喷砂处理,清洁,然后将样品分为4组:G1,浸入标准酸溶液(SAS)中(对照组); G1,浸入标准酸溶液中(对照组)。 G2,浸入丙酮中,然后浸入SAS中; G3,浸入丙酮中,然后浸入SAS中,然后浸入硝酸中; G4,浸入丙酮中,然后浸入SAS中,然后浸入硫酸中。使用粗糙度测试仪确定粗糙度参数,并使用方差分析和Tukey检验(α= 5%)对数据进行统计分析。结果:关于粗糙度参数,没有发现显着差异。扫描电子显微镜和原子力显微镜显示不规则的表面,并且均匀地沉积在表面上。结论:为所有组创建了相似的粗糙度模式。图像和地形图表明,所有组均显示出高水平的粗糙度。

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