首页> 外文期刊>ECS Journal of Solid State Science and Technology >CNC Synthesis from Cellulose Macromolecule and Fabrication of PVA/TiO2/CNC Bio-Nanocomposite Thin Film for Biomedical Applications
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CNC Synthesis from Cellulose Macromolecule and Fabrication of PVA/TiO2/CNC Bio-Nanocomposite Thin Film for Biomedical Applications

机译:纤维素高分子数控合成及PVA/TiO2/CNC生物纳米复合薄膜的制备及其在生物医学领域的应用

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摘要

PolyVinyl Alcohol (PVA) based films with varying concentrations of Cellulose Nano Crystals (CNC) and Titanium dioxide (TiO2) have been prepared and characterised in this study to determine their applications in the biomedical field. Biophysical, microscopic and mechanical property characterization of the films - PVA/CNC/T-0.5, PVA/CNC/T-1.0 and PVA/CNC/T-1.5 were performed. The CNC were extracted from pea peel waste fibres (PPWF) which are rich in cellulose macromolecule (Mol Wt > 5000 da) by adopting acid hydrolysis method. Through Scanning Electron Microscope (SEM) and Fourier Transform Infrared Spectroscopy (FTIR) analysis, uniform distribution and successful incorporation of CNC and TiO2 in the films have been confirmed. From the X-ray diffraction pattern of the films, it could be noted that the crystallinity increased in the films with the addition of CNC and rutile TiO2 in the PVA. The tensile strength of the films also greatly improved with the CNC reinforcement and increase in TiO2 content in the films. Overall, the results of this study suggest that the PVA/CNC/ TiO2 films have the potential to find their application in biomedical devices, especially to be used as a footprint of an ultrasound transducer.
机译:本研究制备了具有不同浓度的纤维素纳米晶体 (CNC) 和二氧化钛 (TiO2) 的聚乙烯醇 (PVA) 基薄膜,以确定它们在生物医学领域的应用。对PVA/CNC/T-0.5、PVA/CNC/T-1.0和PVA/CNC/T-1.5薄膜进行了生物物理、微观和机械性能表征。采用酸解法从富含纤维素大分子(Mol Wt > 5000 da)的豌豆皮废纤维(PPWF)中提取CNC。通过扫描电子显微镜(SEM)和傅里叶变换红外光谱(FTIR)分析,证实了CNC和TiO2在薄膜中的均匀分布和成功掺入。从薄膜的X射线衍射图可以看出,随着CNC和金红石型TiO2的加入,薄膜中的结晶度增加。随着CNC的增强和薄膜中TiO2含量的增加,薄膜的拉伸强度也大大提高。总体而言,本研究结果表明,PVA/CNC/TiO2薄膜具有在生物医学设备中的应用潜力,特别是用作超声换能器的封装。

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