Anhydrous Magnesium Sulfate Mediated Solvent-Free Synthesis of Dihydropyrimidin-2(1H)-ones at Ambient Temperature

D. M. Pore; U. V. Desai; J. S. Thopate

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Anhydrous Magnesium Sulfate Mediated Solvent-Free Synthesis of Dihydropyrimidin-2(1H)-ones at Ambient Temperature

机译：在室温下无水硫酸镁介导的无溶剂合成二氢嘧啶-2（1H）-

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摘要

An anhydrous magnesium sulfate mediated solvent-free protocol is described for the synthesis of dihydropyrimidinones (Biginelli compounds) at ambient temperature.

机译：描述了一种在环境温度下合成二氢嘧啶酮（Biginelli化合物）的无水硫酸镁介导的无溶剂方案。

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《Australian Journal of Chemistry: A Journal for the Publication of Original Research in All Branches of Chemistry》 |2007年第6期|共4页
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D. M. Pore; U. V. Desai; J. S. Thopate;
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正文语种 eng
中图分类化学;
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1. Anhydrous Magnesium Sulfate Mediated Solvent-Free Synthesis of Dihydropyrimidin-2(1H)-ones at Ambient Temperature [J] . D. M. Pore, U. V. Desai, J. S. Thopate Australian Journal of Chemistry: A Journal for the Publication of Original Research in All Branches of Chemistry . 2007,第6期

机译：在室温下无水硫酸镁介导的无溶剂合成二氢嘧啶-2（1H）-
2. Rice husk SiO2 (NPs) supported-BO3H3: a highly active, solvent-free and recyclable catalyst to dihydropyrimidin-2(1H)ones-(thiones) and coumarin-3-carboxylic acid synthesis [J] . Khatavi S. Y., Kantharaju K., Yamanappa H., Current Science: A Fortnightly Journal of Research . 2019,第11期

机译：稻壳SiO2（NPS）支持-BO3H3：对二氢嘧啶-2（1H）的高活性，无溶剂和可回收的催化剂 - （1H） - （象限）和香豆素-3-羧酸合成
3. Copper(II) trifluoroacetate catalyzed synthesis of 3,4- dihydropyrimidin-2(1H)-ones under solvent-free conditions [J] . Dailei Song, Runxia Wang, Yongli Chen, Reaction Kinetics and Catalysis Letters . 2008,第2期

机译：三氟乙酸铜（II）在无溶剂条件下催化合成3,4-二氢嘧啶-2（1H）-酮
4. Coaled carbon-based solid acid: A new and efficient catalyst for click synthesis of 3,4-dihydropyrimidin-2(1H)-ones under solvent-free conditions [C] . Liu Wanyi, Ning Liu, Ruiyuan Zheng, International Conference on Chemical, Material and Metallurgical Engineering . 2013

机译：含有碳化碳固体酸：在无溶剂条件下单击合成3,4-二氢嘧啶-2（1H）酮的新增有效的催化剂
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. Zeolite catalyzed solvent-free one-pot synthesis of dihydropyrimidin-2(1H)-ones – A practical synthesis of monastrol [O] . Mukund G Kulkarni, Sanjay W Chavhan, Mahadev P Shinde, 2009

机译：沸石催化的无溶剂一锅合成二氢嘧啶-2（1H）-酮类化合物-菊酯的实用合成
7. Zeolite catalyzed solvent-free one-pot synthesis of dihydropyrimidin-2(1H)-ones – A practical synthesis of monastrol [O] . Kulkarni, Mukund G, Chavhan, Sanjay W, Shinde, Mahadev P, 2009

机译：沸石催化的无溶剂一锅合成二氢嘧啶-2（1H）-酮类化合物-菊酯的实用合成

Anhydrous Magnesium Sulfate Mediated Solvent-Free Synthesis of Dihydropyrimidin-2(1H)-ones at Ambient Temperature

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