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Simultaneous Multielement Determination of Al, As, Cd, Cr, Cu, Fe, Hg, Mn, Ni, Pb, Sn, and Zn in Bulgur Wheat by ICP-OES

机译:ICP-OES法同时测定小麦中的Al,As,Cd,Cr,Cu,Fe,Hg,Mn,Ni,Pb,Sn和Zn

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摘要

Bulgur is one of the oldest cereal-based foods. This study explains the simultaneous determination by the proposed method for toxic elements such as Al, As, Cd, Cr, Cu, Fe, Hg, Mn, Ni, Pb, Sn, and Zn in bulgur by ICP-OES following digestion in a closed-vessel microwave system. The ICP-OES method is used because it is precise, rapid, simple, and accurate for the determination of 12 metals. The technique can be considered useful for the routine analysis of multi-elements in cereals as well as for quality control purposes. The obtained results in the bulgur samples (mean in mg kg(-1)) were: Al 0.81, Cr 0.19, Cu 3.80, Fe 26.75, Mn 13.60, Ni 0.25, Pb 0.23, Sn 0.17, and Zn 14.30. The concentrations of As, Cd, and Hg were below the detection limits. A certified reference material was used to verify the accuracy of the studied method. The results were in good agreement with the certified values. The toxic metal concentrations are low and the obtained values are suitable for daily intake. The macro and micro nutrient ranges in bulgar wheat did not exceed the dietary reference intake (DRI). The bulgur produced in Turkey has very low levels of toxic metals, is safe for human consumption, and is a highly nutritional and healthy food source. Bulgur wheat is, therefore, safe for public consumption.
机译:碾碎干小麦是最古老的谷类食品之一。这项研究解释了建议的方法同时进行密闭消解后,通过ICP-OES同时测定小麦中小麦中铝,砷,镉,铬,铬,铜,铁,汞,锰,镍,铅,锡和锌的有毒元素-容器微波系统。之所以使用ICP-OES方法,是因为它可以精确,快速,简单且准确地测定12种金属。该技术可用于谷物中多种元素的常规分析以及质量控制。在小麦样品中获得的结果(均以mg kg(-1)为单位)为:Al 0.81,Cr 0.19,Cu 3.80,Fe 26.75,Mn 13.60,Ni 0.25,Pb 0.23,Sn 0.17和Zn 14.30。砷,镉和汞的浓度低于检测极限。使用经过认证的参考材料来验证所研究方法的准确性。结果与认证值高度吻合。有毒金属浓度低,所获得的值适合每日摄入。保加利亚小麦的宏观和微量营养素范围不超过膳食参考摄入量(DRI)。土耳其生产的碾碎干小麦中的有毒金属含量极低,可以安全地供人类食用,并且是高度营养和健康的食物来源。因此,小麦碾碎小麦可安全用于公众消费。

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