Preparation of Fullerene (C_(60)) Nanowhisker-ZnO Nanocomposites by Heat Treatment and Photocatalytic Degradation of Methylene Blue

摘要

The fullerene (Cm) nanowhisker (FNW) nanoparticles were synthesized by the liquid-liquid interfacial precipitation method using good solvent solutions such as pyridine, benzene and toluene saturated with C_(60) and isopropyl alcohol as a polar solvent. The zinc oxide nanoparticles were synthesized sonochemically by applying ultrasonic irradiation to a mixed aqueous-alcoholic solution of zinc nitrate with sodium hydroxide at room temperature. The heated FNW-ZnO nanocomposites were synthesized in an electric furnace at 700 °C for 2 h. The heated FNW-ZnO nanocomposites were characterized by X-ray diffraction, scanning electron microscopy and transmission election microscopy. In addition, by using UV-visible spectrophotometer, the heated FNW-ZnO nanocomposites were determinable as a catalyst in the photocatalytic degradation of methylene blue. The photocatalytic effect of the heated FNW-ZnO nanocomposites were confirmed as being compared with unheated FNW-ZnO nanocomposites in methylene blue under ultraviolet light at 254 nm.