Hydrothermal Synthesis and Crystal Structure Based on Benzophenone-2,4'-carboxylate and 1,2-Bis(4-pyridyl)ethane

Xiaoshuang Zhou

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Hydrothermal Synthesis and Crystal Structure Based on Benzophenone-2,4'-carboxylate and 1,2-Bis(4-pyridyl)ethane

机译：基于苯甲酮-2,4'-羧酸盐和1,2-双（4-吡啶基）乙烷的水热合成及晶体结构

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Co-crystallization of benzophenone-2,4'-carboxylate and 1,2-bis(4-pyridyl)ethane was synthesized and characterized by X-ray diffraction at the triclinic, space group P-1 with a = 7.443(5), b = 9.293(10), c = 13.131(5) A, β = 79.276(5)°, M_r = 363.36, V = 843.1(8) A~3, D_c = 1.431 g/cm~3, F(000) = 380 and Z = 2. There are one molecule of benzopenone-2,4'-carboxylate and 1,2-bis(4-pyridyl)ethane in the asymmetric unit. The intermolecular hydrogen bonds are observed in the compound.

机译：合成了二苯甲酮-2,4'-羧酸盐和1,2-双（4-吡啶基）乙烷的共结晶，并通过X射线衍射在斜边空间群P-1处进行了X射线衍射表征，a = 7.443（5）， b = 9.293（10），c = 13.131（5）A，β= 79.276（5）°，M_r = 363.36，V = 843.1（8）A〜3，D_c = 1.431 g / cm〜3，F（000）＝ 380且Z ＝ 2。在不对称单元中存在一分子苯并萜烯-2，4′-羧酸酯和1，2-双（4-吡啶基）乙烷。在该化合物中观察到分子间氢键。

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《Asian Journal of Chemistry: An International Quarterly Research Journal of Chemistry》 |2012年第7期|共2页
作者
Xiaoshuang Zhou;
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正文语种 eng
中图分类化学;
关键词
Hydrothermal; Synthesis; Crystal structure; Benzophenone-2; 4'-carboxylate; 1; 2-Bis(4-pyridyl)ethane;

机译：水热;合成;晶体结构;苯甲酮-2;4'-羧酸盐;1;2-双（4-吡啶基）乙烷;
入库时间 2022-08-18 10:17:44

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Hydrothermal Synthesis and Crystal Structure Based on Benzophenone-2,4'-carboxylate and 1,2-Bis(4-pyridyl)ethane

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