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Core-Shell Nanofibers With Fire Retardant Properties Prepared By A Co-Axial Electrospinning Technique

机译:同轴静电纺丝技术制备的具有阻燃性能的核壳纳米纤维

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摘要

A novel composite core-shell nanofibers of polyvinyl acetate) (PVAc) as core incorporated with magnesium oxide nano-particles (MgO NPs) and cellulose acetate (CA) as shell were prepared using co-axial electrospinning technique. Core-shell morphology of the prepared composite nanofibers was confirmed by scanning electron microscope (SEM) and field emission-SEM (FE-SEM) imaging techniques and presence of metal oxide in core-shell nanofibers was confirmed from the energy dispersive X-ray (EDX) analysis. Further, thermal, chemical and mechanical properties of the prepared materials were studied with Fourier transform-infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), tensile measurements, ther-mogravimetry analysis (TGA) and differential scanning calorim-etry (DSC) analysis. Finally, fire retardant properties of the prepared nanofibers were studied by inclined flammability and limited oxygen index (LOI) testing. Higher mechanical strength and enhanced fire resistance was reported from the above thorough analysis and therefore, the prepared material could fit well in fire resistance applicationes.
机译:一种新型复合核壳纳米纤维聚醋酸乙烯酯)(PVAc)为核心与氧化镁纳米粒子(分别以NPs)和醋酸纤维素(CA)壳被准备使用同轴电纺的技术。核壳结构的复合纳米纤维被扫描电子确认显微镜(SEM)和场emission-SEM (FE-SEM)成像技术和金属氧化物的存在核壳纳米纤维被确认的能量色散x射线(EDX)分析。热、化学和机械性能准备材料和傅里叶进行了研究变换红外光谱(FTIR)、粉x射线衍射(XRD)、拉伸测量,ther-mogravimetry分析(TGA)和差扫描calorim-etry (DSC)分析。阻燃性能的准备纳米纤维研究了斜可燃性和有限的氧指数(量)测试。机械强度和增强的耐火性从上面的深入分析和报告吗因此,准备的材料可以适应在防火验证。

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