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Superb catalytic activity of as-green synthesized copper ferrite's thermal decomposition of ammonium perchlorate

机译:精采催化活性为绿色合成铜铁素体的热分解铵氯酸铵

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A simple one step method is employed for the synthesis of CuFe2O4 nanoparticles (NPs) aided by utilizing egg albumin (EA) and aloe vera (AV) as solvents. The samples were characterized using X-ray diffraction (XRD), Field Emission Scanning Electron Microscopy (FE-SEM), Thermo Gravimetric/Differential Thermal Anaysis (TG/DTA), Vibration Sample Magnetometer (VSM) and X-ray Photolectron Spectroscopy (XPS). XRD analysis of the samples sowed the presence of CuFe2O4 and CuO in the samples. The ambient VSM study proved the ferrimagnetism behavior of the CuFe2O4. TG/DTA was used to study the catalytic activity of the CuFe2O4 nanoparticles, the results revealed that a 78 degrees C reduction in the decomposition temperature of Ammonium Perchlorate (AP) was achieved while using 6% CuFe2O4 prepared using a mixed EA-AV and calcinated at 700 degrees C. Hence, CuFe2O4 can be potent catalytic agent in several environmental applications as an efficient catalyst. (C) 2021 Elsevier B.V. All rights reserved.
机译:以鸡蛋白蛋白(EA)和芦荟(AV)为溶剂,采用简单的一步法制备CuFe2O4纳米颗粒(NPs)。利用X射线衍射(XRD)、场发射扫描电子显微镜(FE-SEM)、热重/差热分析(TG/DTA)、振动样品磁强计(VSM)和X射线光电子能谱(XPS)对样品进行了表征。样品的XRD分析表明样品中存在CuFe2O4和CuO。环境VSM研究证实了CuFe2O4的铁磁性行为。TG/DTA用于研究CuFe2O4纳米颗粒的催化活性,结果表明,使用6%的CuFe2O4(使用混合EA-AV制备并在700℃下煅烧),可使高氯酸铵(AP)的分解温度降低78℃。因此,CuFe2O4可以作为一种高效催化剂在多种环境应用中成为有效的催化剂。(c)2021爱思唯尔B.V.保留所有权利。

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