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Hydroxyl-functionalized TiO2@SiO2@Ni/nZVI nanocomposites fabrication, characterization and enhanced simultaneous visible light photocatalytic oxidation and adsorption of arsenite

机译:羟基官能化TiO2 @ SiO2 @ Ni / NZVI纳米复合材料制备,表征和增强的同时可见光光催化氧化和砷酸的吸附

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摘要

In this study, salicylic acid-TiO2@SiO2@Ni/nZVI (SA-NFST) nanocomposites with rich hydroxyl groups were synthesized using in situ surface modified, co-precipitation, and sol-gel methods. A variety of techniques, including scanning electron microscopy (SEM), X-ray powder diffraction (XRD), vibrating sample magnetometer (VSM), transmission electron microscopy (TEM), the point of zero charge (PZC), UV-vis diffuse reflectance spectra (UV-vis), infrared spectroscopy (FTIR), and X-ray photoelectron spectroscopy (XPS), were used to characterize the properties of the nanoparticles.
机译:在该研究中,使用原位表面改性,共沉淀和溶胶 - 凝胶方法合成具有富羟基的水杨酸-TiO2纳米复合材料。 各种技术,包括扫描电子显微镜(SEM),X射线粉末衍射(XRD),振动样品磁力计(VSM),透射电子显微镜(TEM),零电荷点(PZC),UV-VI扩散反射率 光谱(UV-VI),红外光谱(FTIR)和X射线光电子能谱(XPS)用于表征纳米颗粒的性质。

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