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Rapid analysis of taurine in energy drinks using amino acid analyzer and Fourier transform infrared (FTIR) spectroscopy as basis for toxicological evaluation

机译:使用氨基酸分析仪和傅里叶变换红外(FTIR)光谱作为毒理学评估的基础快速分析能量饮料中的牛磺酸

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摘要

So-called energy drinks with very high amounts of taurine (up to 4000 mg/l are usually granted by certificates of exemption) are increasingly offered on the market.To control the currently valid maximum limits of taurine in energy drinks,a simple and rapid analytical method is required to use it routinely in food monitoring.In this article,we describe a fast and efficient analytical method (FTIR-spectroscopy) that is able to reliably characterize and quantify taurine in energy drinks.The determination of taurine in energy drinks by FTIR was compared with amino acid analyzer (ion chromatography with ninhydrin-postcolumn derivatization).During analysis of 80 energy drinks,a median concentration of 3180 mg/l was found in alcohol-free products,314mg/l in energy drinks with spirits,151 mg/l in beer-containing drinks and 305 mg/l in beverages with wine.Risk analysis of these products is difficult due to the lack of valid toxicological information about taurine and its interferences with other ingredients of energy drinks (for example caffeine and alcohol).So far,the high taurine concentrations of energy drinks in comparison to the rest of the diet are scientifically doubtful,as the advertised physiological effects and the value of supplemented taurine are unproven.
机译:市场上越来越多地提供所谓的牛磺酸含量很高的能量饮料(通常通过豁免证书授予的剂量高达4000 mg / l)。要控制当前有效的能量饮料中牛磺酸的最大限量,一种简单而快速的方法食品监测中需要常规使用这种分析方法。本文中,我们描述了一种快速可靠的分析方法(FTIR光谱法),该方法能够可靠地表征和定量能量饮料中的牛磺酸。将FTIR与氨基酸分析仪(用茚三酮-柱后衍生离子色谱法)进行比较。在分析80种能量饮料时,无酒精产品的平均浓度为3180 mg / l,烈酒能量饮料的平均含量为314mg / l,151含啤酒的饮料中的毫克/升和含酒的饮料中的毫克/升。由于缺乏有关牛磺酸及其对其他物质的有效毒理学信息,很难对这些产品进行风险分析r能量饮料的成分(例如咖啡因和酒精)。到目前为止,与其他饮食相比,高能量牛磺酸的能量饮料与其他饮食相比存在疑问,因为尚未证明其所宣传的生理效应和牛磺酸的价值。

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