ОСОБЕННОСТИ ПОЛУЧЕНИЯ И СВОЙСТВА ФАЗ ВЫСОКОГО ДАВЛЕНИЯ АМn3V4O_(12) (А = Са, Се, Sm)

Н. И. Кадырова; Ю. Г. Зайнулин; А. П. Тютюнник

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ОСОБЕННОСТИ ПОЛУЧЕНИЯ И СВОЙСТВА ФАЗ ВЫСОКОГО ДАВЛЕНИЯ АМn3V4O_(12) (А = Са, Се, Sm)

机译：获得和高压阶段AMN3V4O_（12）（A = CA，CE，SM）获得和性质的特征

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摘要

В баротермических условиях (Р = 7.0-9.0 ГПа, t = 700-1100°С) получены перовскитоподобные фазы AMn3V4O_(12) (А = Са, Се, Sm). Рентгенографически установлена кристаллическая структура (пр. гр. ImЗ, Z = 2) и вычислены параметры решеток фаз: CaMn3V4O_(12): а = 7/40824(3) А, SmMn3V4O_(12): а = 7/45280(8) A, CeMn3V4O_(12): а = 7/46965(4) А. Изучены температурные зависимости удельного электросопротивления (10-300 К) и магнитной восприимчивости (2-300 К) синтезированных соединений.

机译：在Barothermatic条件下（P = 7.0-9.0GPa，T = 700-1100℃）获得PeroVSK样AM3V4O_（12）（a = Ca，Ce，Sm）。 X射线是晶体结构（C GR.IMZ，Z = 2），并计算阶段格子的参数：CAMN3V4O_（12）：A = 7/40824（3）A，SMMN3V4O_（12）：a = 7/45280（8）A，Cemn3V4O_（12）：a = 7/46965（4）A.电阻率（10-300k）和合成化合物的磁性敏感性（2-300k）的温度依赖性是研究过。

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来源
《Журнал неорганичесκой химии》 |2017年第1期|共8页
作者
Н. И. Кадырова; Ю. Г. Зайнулин; А. П. Тютюнник;
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Институт химии твердого тела УрО РАН Россия 620219 Екатеринбург ул. Первомайская 91;

Институт химии твердого тела УрО РАН Россия 620219 Екатеринбург ул. Первомайская 91;

Институт химии твердого тела УрО РАН Россия 620219 Екатеринбург ул. Первомайская 91;

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中图分类无机化学;
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высокие давления и температуры; структура; электрические и магнитные свойства;

机译：高压和温度;结构体;电气和磁性;

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机译：高压相AMn3V4O_（12）（A = Ca，Ce，Sm）的特定特征和性质
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机译：示波器Os-121 / Usm-140，Os-121a / Usm-140a，Os-121B / Usm-140B，Os-121D / Usm-140D，Os-122 / Usm-141，Os-122a / Usm-141a 170a， HO2-170a，170aR，HO2-170aR，170B，170BR（Hewlett-packard）1807,1807a，1807R（Hickok）

ОСОБЕННОСТИ ПОЛУЧЕНИЯ И СВОЙСТВА ФАЗ ВЫСОКОГО ДАВЛЕНИЯ АМn3V4O_(12) (А = Са, Се, Sm)

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