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An Investigation of Y3Ba5Cu8O18 Doping with Ag Nanoparticles and Its Application as Superconductor

机译:用Ag纳米粒子掺杂Y3Ba5cu8O18的研究及其作为超导体的应用

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Y3Ba5Cu8O18 superconductors were prepared through a standard solid-state reaction and the structural properties of the samples were studied through XRD and the Rietveld refinement method. The effect of silver nanoparticles doping on the Y3Ba5Cu8O18 superconductors was studied as well. It is known that the size of nanoparticles is increased during aging. Therefore, two batches of samples with 1 and 2 wt% of Ag nanoparticles and the size range of 30, 200, 500, 700, 800, and 1000 nm were prepared. After preparing the samples and observing the Meissner effect, the crystallography, critical current density, critical temperature, magnetic susceptibility, SEM, and EDX experiments of the samples were carried out. The results of the critical current density measurements showed that the sample with 2 wt% Ag nanoparticles and the size of 700 nm has the maximum current density. In both batches of samples, increasing the nanoparticle size to 700 nm led to an increase in the critical current density. The crystallography studies showed that silver nanoparticles do not insert into the superconductor's frame. Actually, they are placed in the samples as a distinct phase.
机译:通过标准固态反应制备Y3Ba5Cu8O18超导体,并通过XRD和RietVeld改进方法研究样品的结构性。还研究了掺杂在Y3Ba5Cu8O18超导体上的银纳米颗粒的效果。已知在老化期间纳米颗粒的尺寸增加。因此,制备两批具有1和2wt%的Ag纳米颗粒的样品和30,200,500,700,800和1000nm的尺寸范围。在制备样品并观察Meissner效应后,进行样品的晶体学,临界电流密度,临界温度,磁性敏感性,SEM和EDX实验。临界电流密度测量结果表明,样品具有2wt%Ag纳米颗粒和700nm的尺寸具有最大电流密度。在两批样品中,将纳米颗粒尺寸增加到700nm导致临界电流密度的增加。结晶学研究表明,银纳米颗粒不会插入超导体的框架中。实际上,它们被放置在样品中作为一个明显的相位。

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