Analytical feasibility of a solvent‐assisted flavour evaporation method for aroma analyses in bread crumb

Pico Joana; Oduber Fernanda; Gómez Manuel; Bernal José

摘要

Abstract >The analysis of bread aroma is essential in order to evaluate its quality as well as to improve it. The use of different methodologies for the analysis of volatile compounds lead to varying results. In the present study, the matrix effect, extraction efficiency, limits of detection and quantification as well as the precision of a proposed solvent‐assisted flavour evaporation methodology were evaluated for the first time and compared with a reference method, both differing in the distillation step. The repeatability (8%) and matrix effect (present in 15 of the 31 compounds) were improved with the proposed method but the extraction efficiencies (average of 52%) and the intermediate precision (15%) were not as required. However, the applicability of the reference method was limited to breads with fat levels 2%. For breads higher in fat, the proposed method represents an alternative for aroma analysis. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“main”XML：Lang =“en”> <标题类型=“main”>摘要</ title> >面包香气的分析至关重要，以评估其质量以及改善它。使用不同方法用于分析挥发性化合物导致不同的结果。在本研究中，第一次评价基质效应，提取效率，检测效率，检测效率，检测效率，拟议的溶剂辅助风味蒸发方法的精度，并与参考方法相比，蒸馏步骤不同。用所提出的方法改善了可重复性（第8％）和基质效果（31种化合物中的15个），但提取效率（平均52％）和中间精度（＆ 15％）不得。然而，参考方法的适用性仅限于脂肪水平的面包。对于脂肪较高的面包，所提出的方法代表了芳香分析的替代方案。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2018年第20期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pico Joana&option=202" target="_blank" rel="nofollow">Pico Joana;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Oduber Fernanda&option=202" target="_blank" rel="nofollow">Oduber Fernanda;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gómez Manuel&option=202" target="_blank" rel="nofollow">Gómez Manuel;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bernal José&option=202" target="_blank" rel="nofollow">Bernal José;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>I.U.CinquimaUniversity of ValladolidValladolid Spain;</p> <p>I.U.CinquimaUniversity of ValladolidValladolid Spain;</p> <p>Food Technology AreaUniversity of ValladolidPalencia Spain;</p> <p>I.U.CinquimaUniversity of ValladolidValladolid Spain;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=bread crumb&option=203" rel="nofollow">bread crumb;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=gas chromatography&option=203" rel="nofollow">gas chromatography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solvent extraction&option=203" rel="nofollow">solvent extraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=volatile compounds&option=203" rel="nofollow">volatile compounds;</a> </p> <div class="translation"> 机译：面包屑;气相色谱;溶剂萃取;挥发性化合物; 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J.,</a> <span>1985</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：测定溶剂黄33，溶剂绿3，合成HC（六氯乙烷）烟气燃烧产物和DEGDN（二乙二醇二硝酸酯）在淡水中浓度的分析方法</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_food-fermentation-industries_thesis/020123168903.html">溶剂辅助风味蒸发法与顶空-固相微萃取法结合分析白酒酒醅中挥发性风味成分</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=宫俐莉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 宫俐莉</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李安军&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李安军</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=孙金沅&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,孙金沅</a> <span> <a href="/journal-cn-9397/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 食品与发酵工业 </a> </span> <span> . 2016</span><span>,第009期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_food-science_thesis/020124148616.html">溶剂萃取/溶剂辅助风味蒸发-气相色谱/质谱联用分析野韭菜花挥发性成分</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨梦云&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 杨梦云</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=郑福平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,郑福平</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=段艳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,段艳</a> <span> <a href="/journal-cn-9417/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 食品科学 </a> </span> <span> . 2011</span><span>,第020期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_analytical-instrumentation_thesis/0201223775861.html">加速溶剂萃取法在烟草香气分析中的应用</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=朱晓兰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 朱晓兰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=黄兰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,黄兰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李盼盼&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李盼盼</a> <span> <a href="/journal-cn-8218/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 分析仪器 </a> </span> <span> . 2011</span><span>,第005期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-tobacco-science_thesis/0201259509060.html">溶剂助蒸馏法在烟草香气成分分析中的应用</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=孙凯健&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 孙凯健</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王美琳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王美琳</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=沈轶&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,沈轶</a> <span> <a href="/journal-cn-6914/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国烟草科学 </a> </span> <span> . 2007</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_cereal-feed-industry_thesis/020122165616.html">米饮料中香气挥发性风味成分分析方法的研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=沈波&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 沈波</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王立&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王立</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=马晓佩&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,马晓佩</a> <span> <a href="/journal-cn-9366/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 粮食与饲料工业 </a> </span> <span> . 2009</span><span>,第010期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-40058_thesis/020222388524.html">溶剂及非溶剂萃取结合GC-O/MS分析威代尔冰酒中的香气物质</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tang Ke&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 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