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首页> 外文期刊>Journal of separation science. >Rapid characterization and identification of the chemical constituents and rat metabolites of Deng‐Zhan‐Xi‐Xin injection using ultra high performance liquid chromatography coupled with quadrupole time‐of‐flight mass spectrometry
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Rapid characterization and identification of the chemical constituents and rat metabolites of Deng‐Zhan‐Xi‐Xin injection using ultra high performance liquid chromatography coupled with quadrupole time‐of‐flight mass spectrometry

机译：用超高效液相色谱法与四极型飞行时间质谱法相结合的邓延XI-XIIN注射素化学成分及大鼠代谢产物的快速表征及鉴定

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Abstract >Deng‐Zhan‐Xi‐Xin injection is a well‐known traditional Chinese medicine prescription for the treatment of cardiovascular and cerebral vessel diseases. However, there have been few reports on its chemical constituents and metabolic pathway, which has blocked its further quality control and studies on its pharmacology and mechanism of action. In this study, an integrative method was established to rapidly explore the chemical constituents and metabolites of Deng‐Zhan‐Xi‐Xin injection using ultra high performance liquid chromatography coupled with quadrupole time‐of‐flight tandem mass spectrometry and the UNIFI? software combined with multiple data processing approaches. As a result, a total of 40 compounds, including 9 flavonoids and 31 phenolic acids were identified or tentatively characterized, and five compounds were first reported in Deng‐Zhan‐Xi‐Xin injection. Under the same analysis conditions, 70 compounds have been detected in rats, including 25 prototypes and 45 metabolites. This was the first systematic research study on the metabolic profiling of Deng‐Zhan‐Xi‐Xin injection. This study provides valuable chemical information for the quality control and research on pharmacology and mechanism of action of Deng‐Zhan‐Xi‐Xin injection. Moreover, it provides a valuable strategy for analyzing the chemical components and metabolites of other traditional Chinese medicine prescriptions. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >邓兆 - 鑫注射是一个着名的中医处方治疗心血管和脑血管疾病。然而，还有很少有关于其化学成分和代谢途径的报道，这阻断了其进一步的质量控制和对其药理学和作用机制的研究。在这项研究中，建立了一种完整的方法，以迅速探索邓志XI-XIN注射的化学成分和代谢物，使用超高效液相色谱法与四极其飞行时间串联质谱和UNIFI耦合？软件结合多种数据处理方法。结果，鉴定了总共40种化合物，包括9种黄酮和31个酚酸，特征在于，在邓志XI-XIN注射中首先报道五种化合物。在相同的分析条件下，在大鼠中检测到70种化合物，包括25种原型和45种代谢物。这是邓兆 - 鑫注射液相识的第一个系统研究研究。本研究为邓志鑫注射注射液的质量控制和药理和机制提供了有价值的化学信息。此外，它提供了分析其他中医处方的化学成分和代谢产物的有价值的策略。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2018年第18期</span><b style="margin: 0 2px;">|</b><span>共14页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guo Xin&option=202" target="_blank" rel="nofollow">Guo Xin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lin Shan&option=202" target="_blank" rel="nofollow">Lin Shan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Peiming&option=202" target="_blank" rel="nofollow">Yang Peiming;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ye Ji&option=202" target="_blank" rel="nofollow">Ye Ji;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Du Jiang&option=202" target="_blank" rel="nofollow">Du Jiang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mu Xuemei&option=202" target="_blank" rel="nofollow">Mu Xuemei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mi Nan&option=202" target="_blank" rel="nofollow">Mi Nan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qi Xiaopo&option=202" target="_blank" rel="nofollow">Qi Xiaopo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lei Huibo&option=202" target="_blank" rel="nofollow">Lei Huibo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Weidong&option=202" target="_blank" rel="nofollow">Zhang Weidong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tian Xinhui&option=202" target="_blank" rel="nofollow">Tian Xinhui;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Interdisciplinary Science Research InstituteShanghai University of Traditional Chinese MedicineShanghai China;</p> <p>Innovation Center of Traditional Chinese MedicineChina State Institute of Pharmaceutical IndustryShanghai China;</p> <p>Innovation Center of Traditional Chinese MedicineChina State Institute of Pharmaceutical IndustryShanghai China;</p> <p>Department of Phytochemistry School of PharmacySecond Military Medical UniversityShanghai China;</p> <p>Yunnan Biovalley Pharmaceutical Co. Ltd.Yunnan China;</p> <p>Innovation Center of Traditional Chinese MedicineChina State Institute of Pharmaceutical IndustryShanghai China;</p> <p>Innovation Center of Traditional Chinese MedicineChina State Institute of Pharmaceutical IndustryShanghai China;</p> <p>Department of Phytochemistry School of PharmacySecond Military Medical UniversityShanghai China;</p> <p>Interdisciplinary Science Research InstituteShanghai University of Traditional Chinese MedicineShanghai China;</p> <p>Interdisciplinary Science Research InstituteShanghai University of Traditional Chinese MedicineShanghai China;</p> <p>Interdisciplinary Science Research InstituteShanghai University of Traditional Chinese MedicineShanghai China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chemical constituents&option=203" rel="nofollow">chemical constituents;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=mass spectrometry&option=203" rel="nofollow">mass spectrometry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=metabolites&option=203" rel="nofollow">metabolites;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=multiple data processing&option=203" rel="nofollow">multiple data processing;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=traditional Chinese medicine&option=203" rel="nofollow">traditional Chinese medicine;</a> </p> <div class="translation"> 机译：化学成分;质谱;代谢物;多数据处理;中医; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025847200.html">Rapid characterization and identification of the chemical constituents and rat metabolites of Deng‐Zhan‐Xi‐Xin injection using ultra high performance liquid chromatography coupled with quadrupole time‐of‐flight mass spectrometry</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guo Xin&option=202" target="_blank" rel="nofollow" class="tuijian_auth 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Xiaoguang Huo</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=霍晓光&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,霍晓光</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liwei Chai&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Liwei Chai</a> <span> <a href="/conference-cn-61564/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 世界中医药学会联合会中药化学专业委员会第五届学术年会暨蒙医药论坛 </a> <span> <span> . 2016</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06130425403408.html">IDENTIFICATION AND CHARACTERIZATION OF PHYTOCHEMICALS/METABOLITES OF DESCHAMPSIA ANTARCTICA EXTRACTS BY LIQUID CHROMATOGRAPHY AND MASS SPECTROMETRY LC-MS/MS AND THEIR USES THEREOF.</a> <b>[P]</b> . <span> 外国专利： <!-- --> IN2009CH02800A </span> <span> . 2011-05-20</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：液相色谱-质谱联用LC-MS / MS鉴定和鉴定南极葡聚糖提取物的植物化学/代谢产物及其用途。 </span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06130419686825.html">AN INTEGRATED SOLID PHASE EXTRACTION COUPLED ULTRA-PERFORMANCE LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (SPE-UPLC-MS) METHOD FOR THE PROFILING OF DXP METABOLITES AND SYSTEM DIAGNOSTICS OF DXP PATHWAY</a> <b>[P]</b> . <span> 外国专利： <!-- 世界知识产权组织专利： --> WO2013133772A1 </span> <span> . 2013-09-12</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：固相萃取-超高效液相色谱-质谱联用（SPE-UPLC-MS）进行DXP代谢产物鉴定和DXP通路的系统诊断 </span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130403885055.html">PROCEDURE FOR THE IDENTIFICATION AND QUANTIFICATION OF THE GLYPHOSATE PRODUCT AND THE METABOLITE OF THE AMINO-METHYL PHOSPHONIC ACID DIRECTLY FROM HONEY, USING AN ANALYTIC EXTRACTION FOLLOWED BY A LIQUID CHROMATOGRAPHY COUPLED TO MASS SPECTROMETRY.</a> <b>[P]</b> . <span> 外国专利： <!-- --> MX2018001637A </span> <span> . 2019-08-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：直接从蜂蜜中鉴定和定量草甘膦产物和代谢产物甲基-甲基膦酸的方法，方法是采用液相色谱-质谱联用后的分析萃取。 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704025847200','4',7,2,1,'',this,24)" class="delivery" prompt="010401" 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