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Simultaneous detection of zinc dimethyldithiocarbamate and zinc ethylenebisdithiocarbamate in cabbage leaves by capillary electrophoresis with inductively coupled plasma mass spectrometry

机译：毛细管电泳与电感耦合等离子体质谱法同时检测白菜叶中白菜叶中的锌二甲基二硫代氨基甲酸酯和乙烯基乙基噻吩

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Abstract > We report a simple and highly sensitive method for the simultaneous detection of trace zinc dimethyldithiocarbamate and zinc ethylenebisdithiocarbamate by capillary electrophoresis with inductively coupled plasma mass spectrometry. Zinc dimethyldithiocarbamate and zinc ethylenebisdithiocarbamate were chelated with trans ‐1,2‐diaminocyclohexane‐ N,N,N′,N′ ‐tetraacetic acid to form a macromolecule complex. Then, these two compounds were separated by α‐cyclodextrin‐modified capillary electrophoresis within 12?min at a separation voltage of 15?kV and measured by inductively coupled plasma mass spectrometry. The developed method is sensitive with detection limit of 1.9 and 3.0?ng Zn/mL for zinc dimethyldithiocarbamate and zinc ethylenebisdithiocarbamate, respectively. By means of ultrasound‐assisted extraction methods, zinc dimethyldithiocarbamate and zinc ethylenebisdithiocarbamate spiked into cabbage leaves were successfully extracted and determined with a relative standard deviation ( n? =?5)?≤?6% and a recovery of 95–107%. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >我们报告了一种简单且高度灵敏的方法，用于同时检测痕量锌二甲基二硫代氨基甲酸和乙烯乙基乙酸锌乙烯基石氨基甲酸乙酯通过具有电感耦合等离子体质谱法的毛细管电泳。将二甲基二硫代氨基甲酸锌和乙烯基石硫代氨基甲酸锌与<I>反式 - 二氨基环己烷 - β螯合，N，N，N'，N'S-乙酸 - 乙酸酯，以形成大分子络合物。然后，将这两种化合物通过α-环糊精改性的毛细管电泳分离在12Ω分钟内以15ΩkV的分离电压并通过电感耦合等离子体质谱测量。开发方法分别对锌二甲基二硫代氨基甲酸锌和乙烯基石硫代氨基甲酸锌的检测限敏感。通过超声辅助的提取方法，成功地提取锌二甲基硫代氨基甲酸锌和乙烯基二硫代氨基甲酸盐和乙烯酰基乙酰硫代氨基甲酸酯，并用相对标准偏差（ N 2 = = =Δ5）测定并测定95-107％。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第19期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Jinfa&option=202" target="_blank" rel="nofollow">Chen Jinfa;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fu Fengfu&option=202" target="_blank" rel="nofollow">Fu Fengfu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Siying&option=202" target="_blank" rel="nofollow">Wu Siying;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Jing&option=202" target="_blank" rel="nofollow">Wang Jing;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Zongwen&option=202" target="_blank" rel="nofollow">Wang Zongwen;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>The Key Laboratory of Environment and HealthUniversities and Colleges in Fujian School of Public Health Fujian Medical UniversityFuzhou P. R. China;</p> <p>Ministry of Education Key Laboratory of Analysis and Detection for Food SafetyFuzhou UniversityFuzhou P. R. China;</p> <p>The Key Laboratory of Environment and HealthUniversities and Colleges in Fujian School of Public Health Fujian Medical UniversityFuzhou P. R. China;</p> <p>The Key Laboratory of Environment and HealthUniversities and Colleges in Fujian School of Public Health Fujian Medical UniversityFuzhou P. R. China;</p> <p>State Key Laboratory of Ecological Pest Control for Fujian and Taiwan Crops College of Plant ProtectionFujian Agriculture and Forestry UniversityFuzhou P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=capillary electrophoresis&option=203" rel="nofollow">capillary electrophoresis;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chelates&option=203" rel="nofollow">chelates;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=inductively coupled plasma mass spectrometry&option=203" rel="nofollow">inductively coupled plasma mass spectrometry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=zinc&option=203" rel="nofollow">zinc;</a> </p> <div class="translation"> 机译：毛细管电泳;螯合物;电感耦合等离子体质谱;锌; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846845.html">Simultaneous detection of zinc dimethyldithiocarbamate and zinc ethylenebisdithiocarbamate in cabbage leaves by capillary electrophoresis with inductively coupled plasma mass spectrometry</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Jinfa&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Chen Jinfa,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fu Fengfu&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Fu Fengfu,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Siying&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Wu Siying,</a> <a href="/journal-foreign-35800/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of separation science. .</a> <span>2017</span><span>,第19期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：毛细管电泳与电感耦合等离子体质谱法同时检测白菜叶中白菜叶中的锌二甲基二硫代氨基甲酸酯和乙烯基乙基噻吩</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/070402774061.html">Detection and identification of rabbit liver metallothionein-2 subisoforms by capillary zone electrophoresis - inductively coupled plasma mass spectrometry and microbore HPLC - electrospray mass spectrometry</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chassaigne H.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Chassaigne H.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Casiot C.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Casiot C.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lobinski R.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Lobinski R.,</a> <a href="/journal-foreign-18938/" target="_blank" rel="nofollow" class="tuijian_authcolor">Analusis: Chimie Analytique - Methodes Physiques d'Analyse .</a> <span>2000</span><span>,第5期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：毛细管区带电泳-电感耦合等离子体质谱和微孔HPLC-电喷雾质谱法检测和鉴定兔肝金属硫蛋白2亚型。</span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704028330243.html">Estimated Contributions of Rooibos Tea to the Daily Manganese and Zinc Intakes Determined in Tea Leaves and Tea Infusions by Inductively Coupled Plasma-Mass Spectrometry</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nombuzo Mabuza&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Nombuzo Mabuza,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Henok H. 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