Electrophoretic deposition strategy for the fabrication of highly stable functionalized silica nanoparticle coatings onto nickel‐titanium alloy wires for selective solid‐phase microextraction

Zhou Shanshan; Wang Huiju; Jin Panxia; Wang Ziyi; Wang Xuemei; Du Xinzhen

摘要

Abstract >A new strategy for the immobilization of phenyl‐functionalized silica nanoparticles onto nickel‐titanium alloy wires is presented. The homogeneous and compact silica nanoparticle coating was achieved on the hydrothermally treated nickel‐titanium wires with large surface area by electrophoretic deposition, and followed by self‐assembled modification of phenyltrichlorosilane. Coupled to high‐performance liquid chromatography with ultraviolet detection, the extraction performance of the fabricated fiber was evaluated using typical aromatic compounds in direct‐immersion mode of solid‐phase microextraction. Due to its high extraction efficiency and good selectivity for ultraviolet filters, the novel fiber was employed to investigate the key factors affecting the extraction of ultraviolet filters. Under the optimized conditions, the proposed method presented linear ranges from 0.05 to 300 μg/L with correlation coefficients higher than 0.999 and limits of detection from 0.005 to 0.058 μg/L. Relative standard deviations were below 4.3 and 5.6% for intraday and interday analyses at the spiking level of 50 μg/L ultraviolet filters with the single fiber, respectively. The proposed method was successfully applied to the selective concentration and sensitive detection of target ultraviolet filters from environmental water samples. Furthermore, the developed fiber can be used at least 200 times, and fabricated in a precisely controllable manner. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >将苯基官能化二氧化硅固定到镍钛合金线上的新策略是提出了。通过电泳沉积在具有大表面积的水热处理的镍钛线上实现均匀和紧凑的二氧化硅纳米粒子涂层，然后通过苯三氯硅烷自组装改性。耦合到高性能液相色谱，具有紫外检测，使用典型的芳族化合物在固相微萃取的直浸模式下评价制造纤维的提取性能。由于其高提取效率和诸如紫外线过滤器的良好选择性，采用新型纤维来研究影响紫外线滤波器提取的关键因素。在优化条件下，所提出的方法呈现线性范围为0.05至300μg/ L，相关系数高于0.999，检测限值为0.005至0.058μg/ L.在具有单纤维的分别为50μg/ L紫外线过滤器的尖峰水平分析，相对标准偏差低于4.3和5.6％。所提出的方法已成功应用于从环境水样中的靶紫外线过滤器的选择性浓度和敏感检测。此外，开发的光纤可以使用至少200次，并以精确可控的方式制造。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第24期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Shanshan&option=202" target="_blank" rel="nofollow">Zhou Shanshan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Huiju&option=202" target="_blank" rel="nofollow">Wang Huiju;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jin Panxia&option=202" target="_blank" rel="nofollow">Jin Panxia;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Ziyi&option=202" target="_blank" rel="nofollow">Wang Ziyi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Xuemei&option=202" target="_blank" rel="nofollow">Wang Xuemei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Du Xinzhen&option=202" target="_blank" rel="nofollow">Du Xinzhen;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>College of Chemistry and Chemical EngineeringNorthwest Normal UniversityLanzhou P. R. China;</p> <p>College of Chemistry and Chemical EngineeringNorthwest Normal UniversityLanzhou P. R. China;</p> <p>College of Chemistry and Chemical EngineeringNorthwest Normal UniversityLanzhou P. R. China;</p> <p>College of Chemistry and Chemical EngineeringNorthwest Normal UniversityLanzhou P. R. China;</p> <p>College of Chemistry and Chemical EngineeringNorthwest Normal UniversityLanzhou P. R. China;</p> <p>College of Chemistry and Chemical EngineeringNorthwest Normal UniversityLanzhou P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrophoretic deposition&option=203" rel="nofollow">electrophoretic deposition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nickel‐titanium alloy wire&option=203" rel="nofollow">nickel‐titanium alloy wire;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=silica nanoparticles&option=203" rel="nofollow">silica nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid‐phase microextraction&option=203" rel="nofollow">solid‐phase microextraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ultraviolet filters&option=203" rel="nofollow">ultraviolet filters;</a> </p> <div class="translation"> 机译：电泳沉积;镍钛合金丝;二氧化硅纳米粒子;固相微萃取;紫外线过滤器; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846558.html">Electrophoretic deposition strategy for the fabrication of highly stable functionalized silica nanoparticle coatings onto nickel‐titanium alloy wires for selective solid‐phase microextraction</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Shanshan&option=202" target="_blank" rel="nofollow" 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and titanium alloy substrates by electrochemical deposition</a> <b>[P]</b> . <span> 外国专利：  US6974532B2 </span> <span> . 2005-12-13</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过电化学沉积在钛和钛合金基底上制备磷酸钙相粘附涂层的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130440241794.html">Method for producing adherent coatings of calcium phosphate phases on titanium and titanium alloy substrates by electrochemical deposition</a> <b>[P]</b> . <span> 外国专利：  US2005000819A1 </span> <span> . 2005-01-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过电化学沉积在钛和钛合金基底上制备磷酸钙相粘附涂层的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130450210060.html">Use of palladium-impregnated deposition to selectively initiate electroless plating of titanium and tungsten alloys for wafer fabrication</a> <b>[P]</b> . <span> 外国专利：  KR20000064359A </span> <span> . 2000-11-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用钯浸渍沉积来选择性地启动用于晶圆制造的钛和钨合金的化学镀 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704025846558','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div 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