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首页> 外文期刊>Journal of separation science. >Simultaneous determination of simazine, cyanazine, and atrazine in honey samples by dispersive liquid–liquid microextraction combined with high‐performance liquid chromatography
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Simultaneous determination of simazine, cyanazine, and atrazine in honey samples by dispersive liquid–liquid microextraction combined with high‐performance liquid chromatography

机译：用分散液 - 液体微萃取结合高性能液相色谱法同时测定蜂蜜样品中蜂蜜样品中的蜂蜜样品

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Abstract > A rapid and simple sample preparation method was developed for simultaneous determination of three triazine herbicides in honey samples. The selected herbicides were extracted from honey samples by ionic liquid dispersive liquid–liquid microextraction, separated on a C <sub>18</sub> column (250?mm × 4.6?mm id, 5?μm) using acetonitrile and H <sub>2</sub> O as the mobile phase with gradient elution, and then detected by high‐performance liquid chromatography. The parameters, such as the type and volume of the extraction and disperser solvent, ion strength, pH, extraction time, and centrifuge time were optimized in order to provide the excellent extraction performance. Good linearity was showed for all the target herbicides over the tested concentration range with correlation coefficient higher than 0.994. Three spiked levels (0.005, 0.05, 0.10?mg/kg) were applied for determination of the recoveries of the targets in honey samples in the range of 80–103% with relative standard deviations not larger than 10.6%. The limits of quantification for the analytes ranged between 1.5 and 4.0?μg/kg. The developed method was applied for determination of the target compounds residues in real samples. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</标题> >快速和简单的样品制备方法是为了同时测定蜂蜜样品中的三种三嗪除草剂。通过离子液体分散液 - 液体微萃取从蜂蜜样品中萃取所选的除草剂，使用乙腈和H <sub在C <sub> 18柱（250×mm×4.6×mm ID，5Ωμm）上分离> 2 </ sub> O作为具有梯度洗脱的流动相，然后通过高效液相色谱检测。优化参数，例如提取和分散器溶剂的类型和体积，离子强度，pH，提取时间和离心时间，以提供优异的提取性能。在测试的浓度范围内显示出良好的线性性，相关系数高于0.994。施用三种掺入水平（0.005,0.05,0.10≤mg/ kg），用于测定蜂蜜样品中靶标的回收率，范围为80-103％，相对标准偏差不大于10.6％。分析物的量化限制范围为1.5和4.0°μg/ kg。施用开发方法用于测定真实样品中的目标化合物残留物。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第19期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tian Hongzhe&option=202" target="_blank" rel="nofollow">Tian Hongzhe;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bai Xuesong&option=202" target="_blank" rel="nofollow">Bai Xuesong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xu Jing&option=202" target="_blank" rel="nofollow">Xu Jing;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Plant Protection CollegeShenyang Agricultural UniversityShenyang China;</p> <p>Plant Protection CollegeShenyang Agricultural UniversityShenyang China;</p> <p>Liaoning entry‐exit inspection and quarantine bureauDalian China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=dispersive liquid–liquid microextraction&option=203" rel="nofollow">dispersive liquid–liquid microextraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=herbicides&option=203" rel="nofollow">herbicides;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=honey&option=203" rel="nofollow">honey;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ionic liquids&option=203" rel="nofollow">ionic liquids;</a> </p> <div class="translation"> 机译：分散液 - 液体微萃取;除草剂;蜂蜜;离子液体; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846491.html">Simultaneous determination of simazine, cyanazine, and atrazine in honey samples by dispersive liquid–liquid microextraction combined with high‐performance liquid chromatography</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tian Hongzhe&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Tian Hongzhe,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bai Xuesong&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Bai Xuesong,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xu Jing&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Xu Jing </a> <a href="/journal-foreign-35800/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of separation science. .</a> <span>2017</span><span>,第19期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用分散液 - 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液体微萃取与气相色谱相结合，用于测定环境水样中的氯苯酚</span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-degree-foreign_mphd_thesis/02061784164.html">Determination of Polycyclic Aromatic Hydrocarbons (PAHs) in Water by Dispersive Liquid-Liquid Microextraction with Gas Chromatography-Mass Spectrometry (DLLME-GC-MS)</a> <b>[D] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ogunkunle, Emmanuel O.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Ogunkunle, Emmanuel O. </a> <span>2018</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：分散液-液微萃取-气相色谱-质谱法（DLLME-GC-MS）测定水中的多环芳烃（PAHs）</span> </p> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-journal-foreign-pmc_detail_thesis/040004638930.html">Solvent demulsification-dispersive liquid-liquid microextraction based on solidification of floating organic drop coupled with ultra-high-performance liquid chromatography-tandem mass spectrometry for simultaneous determination of 13 organophosphate esters in aqueous samples</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qing Luo&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Qing Luo,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shiyu Wang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Shiyu Wang,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Muhammad Adeel&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Muhammad Adeel,</a> <span>-1</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：基于悬浮有机液滴固化的溶剂破乳-分散液-液微萃取-超高效液相色谱-串联质谱法同时测定水溶液中的13种有机磷酸酯</span> </p> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/open-access_resources_thesis/01000130558017.html">Determination of Atrazine and Simazine in Environmental Water Samples by Dispersive Liquid-Liquid Microextraction with High Performance Liquid Chromatography</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qingxiang ZHOU&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Qingxiang ZHOU,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Long PANG&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Long PANG,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guohong XIE&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Guohong XIE,</a> <span>2009</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：高效液相色谱分散液 - 液体微萃取法测定环境水样中的阿特拉津和西亚嗪</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-chromatography_thesis/0201246829797.html">基于脂肪酸的漂浮液滴固化分散液液微萃取-高效液相色谱法联用测定酒类样品中的4-乙基苯酚和4-乙基愈创木酚</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=付博&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 付博</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张吉苹&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张吉苹</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=姜晖&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,姜晖</a> <span> <a href="/journal-cn-14390/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 色谱 </a> </span> <span> . 2016</span><span>,第009期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_detail_thesis/0201293914170.html">分散液-液微萃取结合磁固相萃取用于增香保润剂样品中抗氧化剂的测定</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘春波&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘春波</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨光宇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,杨光宇</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘志华&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘志华</a> <span> <a href="/journal-cn-57080/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 分析科学学报 </a> </span> <span> . 2018</span><span>,第1期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_physical-testing-chemical-analysis-part-bchemical-analysis_thesis/0201212560884.html">固相萃取样品-高效液相色谱-串联质谱法快速测定蜂蜜中26种抗生素</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=钱鸣蓉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 钱鸣蓉</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=章虎&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,章虎</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴俐勤&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,吴俐勤</a> <span> <a href="/journal-cn-7677/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 理化检验-化学分册 </a> </span> <span> . 2010</span><span>,第009期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-chromatography_thesis/0201246833754.html">分散液液微萃取／气相色谱-质谱法测定蜂蜜中六六六和滴滴涕类农药残留</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王东&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王东</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=侯传金&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,侯传金</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=赵尔成&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,赵尔成</a> <span> <a href="/journal-cn-14390/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 色谱 </a> </span> <span> . 2015</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-forensic-medicine_thesis/0201279328525.html">分散液液微萃取-气相色谱串联质谱联用法测定生物样品中艾司西酞普兰</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=管青林&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 管青林</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=解文凯&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,解文凯</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吕晨曦&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,吕晨曦</a> <span> <a href="/journal-cn-293/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 法医学杂志 </a> </span> <span> . 2020</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-2134_thesis/02022404077.html">石墨烯-C18增强的中空纤维液相微萃取-高效液相色谱法测定蜂蜜样品中的氯酚</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=WANG Chun&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . WANG Chun</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王春&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王春</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZANG Xiao-huan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,ZANG Xiao-huan</a> <span> <a href="/conference-cn-2134/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 2014第三届环渤海色谱质谱学术报告会 </a> <span> <span> . 2014</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020312658210.html">牛奶和蜂蜜样品中甲硝唑检测新方法研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈丹&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陈丹</a> <span> . 2013</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120112988420.html">蜂蜜中硝基咪唑类抗生素的检测方法及其样品处理方法</a> <b>[P]</b> . <span> 中国专利： CN113030309A </span> <span> . 2021-06-25</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061202822694.html">一种磁性离子液体结合相关微萃取装置用于复杂样品中微量组分分离方法</a> <b>[P]</b> . <span> 中国专利： CN105617711B </span> <span> . 2018.04.10</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130437612466.html">method for the simultaneous determination of purine derivatives and pirimidine, amino acid n - acetylated and dicarbossilici acids in a biological sample by high-performance liquid chromatography (hplc) and high-performance on kit.</a> <b>[P]</b> . <span> 外国专利： <!-- --> ITRM20050085A1 </span> <span> . 2006-09-01</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：高效液相色谱法（hplc）和高性能试剂盒同时测定生物样品中嘌呤衍生物和嘧啶，氨基酸正乙酰化和二碳碳硅酸的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130405906557.html">Method of determination for natural honey using ultra-high performance liquid chromatography</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR101859686B1 </span> <span> . 2018-05-24</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：超高效液相色谱法测定天然蜂蜜的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130408651246.html">Method of determination for natural honey using ultra-high performance liquid chromatography</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR20170116847A </span> <span> . 2017-10-20</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：超高效液相色谱法测定天然蜂蜜的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704025846491','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p class="current">目前支持订阅全部北京大学中文核心（2020）期刊目录。</p> <div style="display: flex;margin-top: 69px;justify-content: space-between;"> <div class="no-sub" 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