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首页> 外文期刊>Journal of separation science. >Directly‐coupled‐column ultra‐fast liquid chromatography with diode array detection method for the rapid quantification of allergenic disperse dyes in water preconcentrated by magnetic solid‐phase extraction
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Directly‐coupled‐column ultra‐fast liquid chromatography with diode array detection method for the rapid quantification of allergenic disperse dyes in water preconcentrated by magnetic solid‐phase extraction

机译：直接耦合柱超快速液相色谱，具有二极管阵列检测方法，用于快速定量过敏性分散染料在水中的磁性相 - 相萃取预浓缩

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Abstract >A directly‐coupled‐column ultra‐fast liquid chromatography coupled with diode array detection method for the determination of 12 allergenic disperse dyes in river water at sub‐ppb levels has been developed and successfully validated. The analytical method is based on the use of two different reversed‐phased columns connected through a two‐position switching valve. A baseline separation was achieved by proper selection of stationary phases, mobile phases, and the use of a gradient elution in both dimensions. Furthermore, an easy‐to‐handle magnetic solid‐phase extraction procedure was developed for the preconcentration of 12 allergenic disperse dyes from river water. An enrichment factor of 100 times was obtained. The results showed excellent performance in terms of trueness (76.8–99.0%), precision (intraday: 2.2–8.0%, interday: 3.3–8.2%), and sensitivity (limits of determination, 0.027–1.46?μg/L). Twenty real samples collected from the outfalls in the Yaojiang, Yongjiang and Fenghuajiang estuary were analyzed, and three of the studied compounds were found in one collected sample (12.6?μg/L for disperse blue 7, 11.6?μg/L for disperse blue 106, and 0.22?μg/L for disperse blue 3). </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >直接耦合柱超快速液相色谱，与二极管阵列检测方法相耦合开发并成功验证了亚PPB水平下河水中12例过敏性分散染料的测定。分析方法基于使用通过双位置切换阀连接的两个不同的反相色谱柱。 A baseline separation was achieved by proper selection of stationary phases, mobile phases, and the use of a gradient elution in both dimensions.此外，开发了一种易于处理的磁共相萃取程序，用于从河水中的12个过敏性分散染料的前浓缩。获得了100次的富集因子。结果表现出具有优异的性能（76.8-99.0％），精确度（日内：2.2-8.0％，间期：3.3-8.2％）和敏感性（测定限值，0.027-1.46？μg/ L）。分析了从姚江，永江和奉花江河口的排水口收集的20个真实样品，并在一个收集的样品中发现了三种研究的化合物（用于分散蓝7的12.6ΩΩ·μg/ L.对于分散蓝106分散蓝色3. </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第22期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhan Ping‐Ping&option=202" target="_blank" rel="nofollow">Zhan Ping‐Ping;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Yun&option=202" target="_blank" rel="nofollow">Zhang Yun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Jun‐Chao&option=202" target="_blank" rel="nofollow">Liu Jun‐Chao;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhu Yan&option=202" target="_blank" rel="nofollow">Zhu Yan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhao Yong‐Gang&option=202" target="_blank" rel="nofollow">Zhao Yong‐Gang;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Marine SciencesNingbo UniversityNingbo Zhejiang China;</p> <p>Department of ChemistryZhejiang UniversityHangzhou Zhejiang China;</p> <p>Environment Monitoring Center of ChangzhiChangzhi Shanxi China;</p> <p>Department of ChemistryZhejiang UniversityHangzhou Zhejiang China;</p> <p>Department of ChemistryZhejiang UniversityHangzhou Zhejiang China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=allergenic disperse dyes&option=203" rel="nofollow">allergenic disperse dyes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=enrichment factors&option=203" rel="nofollow">enrichment factors;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=magnetic solid‐phase extraction&option=203" rel="nofollow">magnetic solid‐phase extraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=river water&option=203" rel="nofollow">river water;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ultra‐fast liquid chromatography&option=203" rel="nofollow">ultra‐fast liquid chromatography;</a> </p> <div class="translation"> 机译：过敏性分散染料;富集因子;磁性固相提取;河水;超快速液相色谱; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" 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href="/academic-journal-cn_food-science_thesis/020123953630.html">高效液相色谱-二极管阵列检测器结合固相萃取法快速测定食品中米酵菌酸残留</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李红艳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 李红艳</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=金燕飞&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,金燕飞</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=黄海智&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,黄海智</a> <span> <a href="/journal-cn-9417/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 食品科学 </a> </span> <span> . 2016</span><span>,第024期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_foreign-environmental-science-technology_thesis/0201262196331.html">环境水中微量酚类通过微柱浓缩法用高速液相色谱进行快速测定</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴荣祖&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 吴荣祖</a> <span> <a href="/journal-cn-42178/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 国外环境科学技术 </a> </span> <span> . 1989</span><span>,第001期</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06130406561184.html">QUICK METHOD FOR DETERMINING ORGANOMETALLIC COMPOUNDS IN ULTRA-TRACES, FROM SOIL SAMPLES, BY ULTRASONIC EXTRACTION-HEADSPACE-SOLID PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY COUPLED WITH MASS SPECTROMETRY (): SURFACE WATER, SOIL, AIR, VEGETATION</a> <b>[P]</b> . <span> 外国专利： <!-- --> RO132682A2 </span> <span> . 2018-06-29</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：超声萃取-顶空固相微萃取-质谱联用气相色谱法快速测定土壤样品中痕量有机物的快速方法（）：地表水，土壤，空气，植被 </span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06130419686825.html">AN INTEGRATED SOLID PHASE EXTRACTION COUPLED ULTRA-PERFORMANCE LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (SPE-UPLC-MS) METHOD FOR THE PROFILING OF DXP METABOLITES AND SYSTEM DIAGNOSTICS OF DXP PATHWAY</a> <b>[P]</b> . <span> 外国专利： <!-- 世界知识产权组织专利： --> WO2013133772A1 </span> <span> . 2013-09-12</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：固相萃取-超高效液相色谱-质谱联用（SPE-UPLC-MS）进行DXP代谢产物鉴定和DXP通路的系统诊断 </span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130403885055.html">PROCEDURE FOR THE IDENTIFICATION AND QUANTIFICATION OF THE GLYPHOSATE PRODUCT AND THE METABOLITE OF THE AMINO-METHYL PHOSPHONIC ACID DIRECTLY FROM HONEY, USING AN ANALYTIC EXTRACTION FOLLOWED BY A LIQUID CHROMATOGRAPHY COUPLED TO MASS SPECTROMETRY.</a> <b>[P]</b> . <span> 外国专利： <!-- --> MX2018001637A </span> <span> . 2019-08-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：直接从蜂蜜中鉴定和定量草甘膦产物和代谢产物甲基-甲基膦酸的方法，方法是采用液相色谱-质谱联用后的分析萃取。 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704025846456','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div 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