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首页> 外文期刊>Journal of separation science. >Simultaneous determination of polysaccharides and 21 nucleosides and amino acids in different tissues of Salvia miltiorrhizaSalvia miltiorrhiza from different areas by UV–visible spectrophotometry and UHPLC with triple quadrupole MS/MS
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Simultaneous determination of polysaccharides and 21 nucleosides and amino acids in different tissues of Salvia miltiorrhizaSalvia miltiorrhiza from different areas by UV–visible spectrophotometry and UHPLC with triple quadrupole MS/MS

机译：通过UV可见分光光度法和UHPLC与三重四极孔MS / MS不同地区不同地区的不同面积的不同组织中多糖和21例核苷和氨基酸的同时测定丹参的不同组织中的丹参

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Abstract > Salvia miltiorrhiza , a traditional Chinese medicine, is a widely used herbal medicine to treat cardiovascular and cerebrovascular diseases. In this study, ultraviolet (UV)–visible spectrophotometry and ultra‐high performance liquid chromatography with triple quadrupole tandem mass spectrometry analytical methods were used for rapid quantification of polysaccharides and 21 nucleosides and amino acids in S. miltiorrhiza to determine 17 samples of different tissues from different areas. Based on the total contents, hierarchical clustering analysis and principal components analysis were performed to classify these samples. The established methods were validated with good linearity, precision, repeatability, stability, and recovery. Chemical analysis revealed a higher content of total analytes in the sample of inflorescence from Nanjing (34.17?mg/g), sample of root and rhizome from Shaanxi (34.13?mg/g) and sample of stem and leaf from Nanjing (31.14?mg/g), respectively, indicating that root and rhizome from Shaanxi and the aerial parts from Nanjing exhibited the highest quality due to their highest content. In addition, contents of nucleosides and amino acids in the aerial parts (14.67?mg/g) were much higher than that in roots and rhizomes (9.17?mg/g). This study suggested that UV–visible spectrophotometry and ultra‐high performance liquid chromatography with triple quadrupole tandem mass spectrometry are effective techniques to analyze polysaccharides, nucleosides, and amino acids in plants, and they provided valuable information for the development and utilization value of the aerial parts of S. miltiorrhiza . This analysis would also provide useful information for the quality control of S. miltiorrhiza . </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> > 丹参米蒂希粒子</ i>，中药，是广泛使用的草药治疗心血管和脑血管疾病。在该研究中，使用具有三重四极杆串联质谱分析方法的紫外（UV）可见分光光度法和超高效液相色谱法用于快速定量多糖和21核苷和氨基酸。 Miltiorrhiza </ i>以确定来自不同区域的17个不同组织的样本。基于总内容，进行分层聚类分析和主成分分析以对这些样本进行分类。已建立的方法以良好的线性，精度，可重复性，稳定性和恢复验证。化学分析揭示了南京（34.17μmg/ g），从陕西（34.13Ωmg/ g），根和根茎样品和从南京的茎和叶样品（31.14Ω·mg / g）分别表明来自陕西的根和根茎和来自南京的空中零件由于其最高含量而表现出最高质量。此外，空中部件（14.67Ω·mg / g）中核苷和氨基酸的含量远高于根和根茎（9.17μmg/ g）。本研究表明，UV可见分光光度法和超高效液相色谱法与三重四极杆串联质谱法是分析植物中多糖，核苷和氨基酸的有效技术，并为空中的开发和利用价值提供了有价值的信息 s的部分。 Miltiorrhiza </ i>。该分析还将提供用于 S的质量控制的有用信息。 Miltiorrhiza </ i>。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2018年第5期</span><b style="margin: 0 2px;">|</b><span>共13页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xiang Xiang&option=202" target="_blank" rel="nofollow">Xiang Xiang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sha Xiuxiu&option=202" target="_blank" rel="nofollow">Sha Xiuxiu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Su Shulan&option=202" target="_blank" rel="nofollow">Su Shulan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhu Zhenhua&option=202" target="_blank" rel="nofollow">Zhu Zhenhua;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guo Sheng&option=202" target="_blank" rel="nofollow">Guo Sheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yan Hui&option=202" target="_blank" rel="nofollow">Yan Hui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qian Dawei&option=202" target="_blank" rel="nofollow">Qian Dawei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Duan Jin‐ao&option=202" target="_blank" rel="nofollow">Duan Jin‐ao;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> <p>Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources IndustrializationNanjing University of Chinese MedicineNanjing China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=amino acids&option=203" rel="nofollow">amino acids;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nucleosides&option=203" rel="nofollow">nucleosides;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polysaccharides&option=203" rel="nofollow">polysaccharides;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=traditional Chinese medicine&option=203" rel="nofollow">traditional Chinese medicine;</a> </p> <div class="translation"> 机译：氨基酸;核苷;多糖;中医; </div> </li> <li> <span class="lefttit">入库时间</span> <span>2022-08-20 10:07:47</span> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846414.html">Simultaneous determination of polysaccharides and 21 nucleosides and amino acids in different tissues of <i >Salvia miltiorrhizaSalvia miltiorrhiza from different areas by 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2013</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_fujian-analysis-testing_thesis/0201211840846.html">用ICP-MS法测定四个不同地区泽泻中微量元素的含量</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=邱招钗&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 邱招钗</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨妙峰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,杨妙峰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=何鹰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,何鹰</a> <span> <a href="/journal-cn-7656/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 福建分析测试 </a> </span> <span> . 2003</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" 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target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 侯冬岩</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=回瑞华&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,回瑞华</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李铁纯&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李铁纯</a> <span> <a href="/conference-cn-31987/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国物理学会第六届质谱分会会员代表大会暨学术报告会 </a> <span> <span> . 2000</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020311498736.html">不同地区肾结石患者血清和尿液微量元素水平ICP-MS测定及比较</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨盛华&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 杨盛华</a> <span> . 2011</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. 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</span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130436823039.html">Simultaneous screening for multiple organic acids, amino acids and glycines using GC/MS</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR100600900B1 </span> <span> . 2006-07-13</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用GC / MS同时筛选多种有机酸，氨基酸和甘氨酸 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130446031183.html">Simultaneous screening for multiple organic acids amino acids and glycines using GC/MS</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR20020084610A </span> <span> . 2002-11-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用GC / MS同时筛选多种有机氨基酸，甘氨酸 </span> </p> </li> 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