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首页> 外文期刊>Journal of separation science. >Deep eutectic solvent based magnetic nanofluid in the development of stir bar sorptive dispersive microextraction: An efficient hyphenated sample preparation for ultra‐trace nitroaromatic explosives extraction in wastewater
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Deep eutectic solvent based magnetic nanofluid in the development of stir bar sorptive dispersive microextraction: An efficient hyphenated sample preparation for ultra‐trace nitroaromatic explosives extraction in wastewater

机译：搅拌棒吸附分散微萃取的深度共晶溶剂基磁性纳米流体：废水中超痕量硝基氨爆炸物提取的高效连锁样品制剂

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Abstract > A deep eutectic solvent based magnetic nanofluid was coupled with stir bar sorptive dispersive microextraction as a hyphenated sample preparation technique. The neodymium core magnetic stir bar was coated physically with nanofluid of magnetic carbon nanotube nanocomposites and deep eutectic solvents. The prepared nanofluid has magnetic and strong sorbing properties and is compatible with gas chromatography. In this nanofluid, the deep eutectic solvent acts simultaneously as both carrier and stabilizer for magnetic nanotubes. The predominant experimental variables affecting the extraction efficiency of nitroaromatic compounds were evaluated. Under the optimized conditions, the limit of detection and enrichment factor were in the range of 0.2–4.9?ng/L and 852–1480, respectively. The relative standard deviations were between 5.6 and 10.2% ( n? =?6). Method validation was performed by both spiking–recovery method and comparison of results with other methods. Finally, the proposed method was successfully applied for the extraction and pre‐concentration of nitroaromatic explosives in water samples, followed by determination by gas chromatography with micro‐electron capture detection. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >深凝胶基溶剂基磁性纳米流体与搅拌棒吸附分散微萃取为连键样品制备技术。用磁性碳纳米管纳米复合材料和深凝胶溶剂的纳米流体和深层溶剂物理涂覆钕芯磁搅拌棒。制备的纳米流体具有磁性和强大的吸附性能，与气相色谱相容。在该纳米流体中，深度共晶溶剂同时用作磁性纳米管的载体和稳定剂。评价影响硝基芳族化合物提取效率的主要实验变量。在优化的条件下，检测和富集因子的极限分别为0.2-4.9≤ng/ l和852-1480。相对标准偏差在5.6和10.2％之间（ n = = =Δ6）。方法验证是通过Spiking恢复方法进行的，并与其他方法的结果进行比较。最后，该方法成功地应用于水样中的硝基芳族炸药的提取和预浓度，然后通过气相色谱法测定微型电子捕获检测。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第24期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zarei Ali Reza&option=202" target="_blank" rel="nofollow">Zarei Ali Reza;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nedaei Maryam&option=202" target="_blank" rel="nofollow">Nedaei Maryam;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ghorbanian Sohrab Ali&option=202" target="_blank" rel="nofollow">Ghorbanian Sohrab Ali;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemistry Faculty of Chemistry and Chemical EngineeringMalek Ashtar University of TechnologyTehran Iran;</p> <p>Department of Chemistry Faculty of Chemistry and Chemical EngineeringMalek Ashtar University of TechnologyTehran Iran;</p> <p>Faculty of Chemical Engineering School of EngineeringUniversity of TehranTehran Iran;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=bucky gel&option=203" rel="nofollow">bucky gel;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=carbon nanotubes&option=203" rel="nofollow">carbon nanotubes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanofluids&option=203" rel="nofollow">nanofluids;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nitroaromatics&option=203" rel="nofollow">nitroaromatics;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=wastewater&option=203" rel="nofollow">wastewater;</a> </p> <div class="translation"> 机译：Bucky凝胶;碳纳米管;纳米流体;硝基甲族;废水; </div> </li> </ul> </div> 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